Effect of an abrupt change growth velocity on directionally solidified microstructures of Ni-24.19 wt%Nb hypereutectic alloy

Microstructure evolution of Ni-24.19 wt%Nb hypereutectic alloys was investigated to develop a method to increase the productivity of in situ composite in directional solidification. The results show that at the constant growth velocity of 10 mu m/s, coarse primary beta-Ni3Nb plate dendrites were firstly precipitated from the liquid. However, at the growth velocity changing abruptly from 1 mu m/s to 10 mu m/s, only coupled growth eutectics were observed in the solidification microstructure. The coupled eutectic growth stable at 10 mu m/s is possibly ascribed to the interface growth temperature of coupled eutecitc exceeding that of beta-Ni3Nb single phase. Another probable factor to permit the coupled eutectic growth stable at 10 mu m/s is the difficult nucleation of beta-Ni3Nb phase in front of the eutectic growth interface. By changing solidification process, the productivity for the formation of in situ composite of Ni-24.19 wt%Nb hypereutectic alloy is improved by a factor of 5. (C) 2007 Elsevier BN. All rights reserved.