X-ray diffraction study of the structure of detonation nanodiamonds

被引：31
作者：
Ozerin, A. N. [1 ]
Kurkin, T. S. [1 ]
Ozerina, L. A. [1 ]
Dolmatov, V. Yu. [2 ]
机构：
[1] Russian Acad Sci, Inst Synthet Polymer Mat, Moscow 117393, Russia
[2] Joint Stock Co, Diamond Ctr, St Petersburg 193076, Russia
来源：
CRYSTALLOGRAPHY REPORTS | 2008年 / 53卷 / 01期
基金：
俄罗斯基础研究基金会;
关键词：
D O I：
10.1134/S1063774508010070
中图分类号：
O7 [晶体学];
学科分类号：
0702 ; 070205 ; 0703 ; 080501 ;
摘要：
The spatial structure of aggregates formed by detonation nanodiamonds is investigated using the wide-angle and small-angle X-ray scattering techniques. The effective sizes of crystallites and the crystallite size distribution function are determined. The shape of scattering aggregates is restored from the small-angle X-ray scattering data. An analysis of the results obtained allowed the conclusion that the nanodiamond aggregates have an extended spatial structure composed of nine to ten clusters, each involving four to five crystallites with a crystal lattice of the diamond type.
引用
收藏
页码：60 / 67
页数：8
相关论文
共 23 条
  • [11] Automated matching of high- and low-resolution structural models
    Kozin, MB
    Svergun, DI
    [J]. JOURNAL OF APPLIED CRYSTALLOGRAPHY, 2001, 34 : 33 - 41
  • [12] Unusually tight aggregation in detonation nanodiamond:: Identification and disintegration
    Krüger, A
    Kataoka, F
    Ozawa, M
    Fujino, T
    Suzuki, Y
    Aleksenskii, AE
    Vul', AY
    Osawa, E
    [J]. CARBON, 2005, 43 (08) : 1722 - 1730
  • [13] Surface chemistry of nanodiamonds
    Kulakova, II
    [J]. PHYSICS OF THE SOLID STATE, 2004, 46 (04) : 636 - 643
  • [14] SCATTERING FROM FRACTALS
    MARTIN, JE
    HURD, AJ
    [J]. JOURNAL OF APPLIED CRYSTALLOGRAPHY, 1987, 20 (02) : 61 - 78
  • [15] NEVEROVSKAYA AY, 2004, FIZ TVERD TELA, V46, P646
  • [16] [Озерин А.Н. Ozerin A.N.], 2006, [Доклады Академии наук, Doklady Akademii nauk], V411, P71
  • [17] OZERIN AN, 1984, VYSOKOMOL SOEDIN A+, V26, P394
  • [18] The spatial structure of dendritic macromolecules
    Ozerin, AN
    Svergun, DI
    Volkov, VV
    Kuklin, AI
    Gordelyi, VI
    Islamov, AK
    Ozerina, LA
    Zavorotnyuk, DS
    [J]. JOURNAL OF APPLIED CRYSTALLOGRAPHY, 2005, 38 : 996 - 1003
  • [19] OZERIN AN, 1986, ZAVODSK LAB, V52, P20
  • [20] Optical properties and structure of nanodiamonds
    Raty, JY
    Galli, G
    [J]. JOURNAL OF ELECTROANALYTICAL CHEMISTRY, 2005, 584 (01): : 9 - 12
123