Magnet design with high B0 homogeneity for fast-field-cycling NMR applications

被引:55
作者
Lips, O [1 ]
Privalov, AE
Dvinskikh, SV
Fujara, F
机构
[1] Tech Univ Darmstadt, Fachbereich Phys, D-64289 Darmstadt, Germany
[2] St Petersburg State Univ, Inst Phys, St Petersburg 198904, Russia
关键词
D O I
10.1006/jmre.2000.2279
中图分类号
Q5 [生物化学];
学科分类号
071010 ; 081704 ;
摘要
The design, construction, and performance of a low-inductance solenoidal coil with high B-0 homogeneity for fast-field-cycling NMR is presented. It consists of six concentric layers. The conductor width is varied to minimize the B-0 inhomogeneity in the volume of the sample. This is done using an algorithm which takes the real shape of the conductor directly into account. The calculated coil geometry can be manufactured easily using standard computerized numeric control equipment, which keeps the costs low. The coil is liquid cooled and produces a B-0 field of 0.95 T at 800 A. The field inhomogeneity in a cylindrical volume (diameter 5 mm, length 10 mm) is about 10 ppm, and the inductance is 190 muH. Switching times below 200 mus can be achieved. During 6 months of operation the coil has shown good stability and reliability. (C) 2001 Academic Press.
引用
收藏
页码:22 / 28
页数:7
相关论文
共 26 条
[11]   B-11 IMAGING WITH FIELD-CYCLING NMR AS A LINE NARROWING TECHNIQUE [J].
LEE, Y ;
MICHAELS, DC ;
BUTLER, LG .
CHEMICAL PHYSICS LETTERS, 1993, 206 (5-6) :464-466
[12]  
Montgomery D.B., 1969, SOLENOID MAGNET DESI
[14]  
Noack F., 1997, ANNU REP NMR SPECTRO, V33, P1
[15]   Coil design for large-volume high-B-1 homogeneity for solid-state NMR applications [J].
Privalov, AF ;
Dvinskikh, SV ;
Vieth, HM .
JOURNAL OF MAGNETIC RESONANCE SERIES A, 1996, 123 (02) :157-160
[16]   Frequency-dependent spin-lattice relaxation study of transport processes in superionic conductors [J].
Privalov, AF ;
Dvinskikh, SV ;
Fujara, F ;
Vieth, HM .
APPLIED MAGNETIC RESONANCE, 1998, 15 (3-4) :353-361
[17]   PRECISION HIGH SPEED CURRENT REGULATORS FOR OCCASIONALLY SWITCHED INDUCTIVE LOADS [J].
REDFIELD, AG ;
FITE, W ;
BLEICH, HE .
REVIEW OF SCIENTIFIC INSTRUMENTS, 1968, 39 (05) :710-&
[18]   A POWERFUL NMR FIELD-CYCLING DEVICE USING GTOS AND MOSFETS FOR RELAXATION DISPERSION AND ZERO-FIELD STUDIES [J].
ROMMEL, E ;
MISCHKER, K ;
OSSWALD, G ;
SCHWEIKERT, KH ;
NOACK, F .
JOURNAL OF MAGNETIC RESONANCE, 1986, 70 (02) :219-234
[19]   A HIGH-FIELD AIR-CORED MAGNET COIL DESIGN FOR FAST-FIELD-CYCLING NMR [J].
SCHWEIKERT, KH ;
KRIEG, R ;
NOACK, F .
JOURNAL OF MAGNETIC RESONANCE, 1988, 78 (01) :77-96
[20]  
SOUSA DM, 1997, P 7 EUR C POW EL APP, V2