Growth by free evaporation method and physico - chemical properties of calcium succinate single crystals

被引：2
作者：
Christy, D. S. [1 ]
Mahadevan, C. K. [1 ]
Shajan, X. Sahaya [1 ]
机构：
[1] PSN Coll Engn & Technol, Sch Basic Engn Sci, Tirunelveli 627152, Tamil Nadu, India
来源：
OPTIK | 2017年 / 145卷
关键词：
Crystal growth; Powder X-ray diffraction; Thermal analysis; NLO material; Microhardness; Dielectric properties; BEHAVIOR;
D O I：
10.1016/j.ijleo.2017.07.065
中图分类号：
O43 [光学];
学科分类号：
070207 ; 0803 ;
摘要：
Calcium succinate single crystals were grown by adopting the free evaporation method for the first time and characterized. Powder X-ray diffraction, FTIR spectral and thermo-gravimetric measurements were carried out to characterize the grown crystals structurally, chemically and thermally. Optical characterization has been done by UV-vis-NIR spectral and second harmonic generation efficiency measurements. Microhardness and dielectric measurements were carried out to characterize mechanically and electrically. The results obtained indicate that the grown crystals exhibit good crystallinity, triclinic lattice structure, reasonable thermal stability (up to 68 degrees C), good transmittance (in the wavelength range from 240 to 1200 nm), second harmonic generation, mechanical softness and normal dielectric behavior. (C) 2017 Elsevier GmbH. All rights reserved.
引用
收藏
页码：418 / 427
页数：10
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