Determination of the total unsaturation in vegetable oils by Fourier transform Raman spectroscopy and multivariate calibration

被引:76
作者
Barthus, RC [1 ]
Poppi, RJ [1 ]
机构
[1] Univ Estadual Campinas, Inst Quim, BR-13083970 Campinas, SP, Brazil
关键词
vegetable oils; NIR-FT Raman spectroscopy; multivariate calibration;
D O I
10.1016/S0924-2031(01)00107-2
中图分类号
O65 [分析化学];
学科分类号
070302 ; 081704 ;
摘要
In this paper multivariate calibration was used in conjunction with NIR-Fourier transform Raman spectroscopy for determination of the total degree of unsaturation in vegetable oils. For this purpose, different vegetable oils and some mixtures were employed as calibration standards. A calibration model based on partial least squares (PLS) was constructed and used to analyse oils with iodine values ranging from 17 to 130. This methodology is rapid, simple and can be easily used in quality control laboratories or to monitor industrial process on line. (C) 2001 Elsevier Science B.V. All rights reserved.
引用
收藏
页码:99 / 105
页数:7
相关论文
共 9 条
[1]  
*AM OIL CHEM SOC, 1989, OFF METH REC PRACT A
[2]   Feasibility of measuring blood glucose concentration by near-infrared Raman spectroscopy [J].
Berger, AJ ;
Itzkan, I ;
Feld, MS .
SPECTROCHIMICA ACTA PART A-MOLECULAR AND BIOMOLECULAR SPECTROSCOPY, 1997, 53 (02) :287-292
[3]  
*CAMOAS, 1996, UNSCR 6 0
[4]   DETERMINATION OF OCTANE NUMBERS AND REID VAPOR-PRESSURE OF COMMERCIAL PETROLEUM FUELS USING FT-RAMAN SPECTROSCOPY AND PARTIAL LEAST-SQUARES REGRESSION-ANALYSIS [J].
COOPER, JB ;
WISE, KL ;
GROVES, J ;
WELCH, WT .
ANALYTICAL CHEMISTRY, 1995, 67 (22) :4096-4100
[5]   The applications of Raman spectroscopy in food science [J].
LiChan, ECY .
TRENDS IN FOOD SCIENCE & TECHNOLOGY, 1996, 7 (11) :361-370
[6]  
MARTEBS H, 1989, MULTIVARIATE CALIBRA
[7]   QUANTITATIVE-ANALYSIS OF OILS AND FATS BY FOURIER-TRANSFORM RAMAN-SPECTROSCOPY [J].
SADEGHIJORABCHI, H ;
WILSON, RH ;
BELTON, PS ;
EDWARDSWEBB, JD ;
COXON, DT .
SPECTROCHIMICA ACTA PART A-MOLECULAR AND BIOMOLECULAR SPECTROSCOPY, 1991, 47 (9-10) :1449-1458
[8]   Univariate and multivariate calibration for the quantitative determination of methyl-parathion in pesticide formulations by FT-Raman spectroscopy [J].
Skoulika, SG ;
Georgiou, CA .
APPLIED SPECTROSCOPY, 2000, 54 (05) :747-752
[9]   RAPID AND DIRECT IODINE VALUE AND SAPONIFICATION NUMBER DETERMINATION OF FATS AND OILS BY ATTENUATED TOTAL REFLECTANCE FOURIER-TRANSFORM INFRARED-SPECTROSCOPY [J].
VANDEVOORT, FR ;
SEDMAN, J ;
EMO, G ;
ISMAIL, AA .
JOURNAL OF THE AMERICAN OIL CHEMISTS SOCIETY, 1992, 69 (11) :1118-1123