Matrix effect on the analysis of amphenicols in fish by liquid chromatography-tandem mass spectrometry (LC-MS/MS)

被引：3

作者：

Guidi, L. R. ^{[1
]}

Tette, P. A. S. ^{[1
]}

Evangelista, W. P. ^{[1
]}

Fernandes, C. ^{[2
]}

Gloria, M. B. A. ^{[1
]}

机构：

[1] Univ Fed Minas Gerais, Fac Farm, LBqA Lab Bioquim Alimentos, BR-31270901 Belo Horizonte, MG, Brazil

[2] Univ Fed Minas Gerais, Lab Controle Qualidade Medicamentos, Fac Farm, BR-31270901 Belo Horizonte, MG, Brazil

来源：

VII BRAZILIAN CONGRESS ON METROLOGY (METROLOGIA 2013) | 2015年 / 575卷

关键词：

VALIDATION;

D O I：

10.1088/1742-6596/575/1/012036

中图分类号：

O42 [声学];

学科分类号：

070206 ; 082403 ;

摘要：

Matrix effect is an important parameter to be investigated during the development and validation of a method for the quantitative determination of contaminants in food. The objective of this study was to evaluate the matrix effect, through statistical tests, in the quantification of amphenicols in fish by HPLC-MS/MS. The study was performed by comparing the standard curves prepared in solvent solutions and in a fish sample previously known to be free of amphenicols. Since matrix effect was observed for the three analytes, calibration curves for quantification of chloramphenicol, thiamphenicol and florfenicol should be constructed using the matrix.

引用

页数：5

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