Study of crystallization and melting of solid waxes by photometric and thermal methods

被引:2
作者
Shishkin, Yu. L.
Yazynina, I. V.
Ovchar, E. V.
机构
[1] I. M. Gubkin Russian State University of Oil and Gas, Moscow
关键词
Photometry - Data handling;
D O I
10.1007/s10553-008-0003-8
中图分类号
TE [石油、天然气工业]; TK [能源与动力工程];
学科分类号
0807 ; 0820 ;
摘要
The crystallization temperature and melting point of individual waxes and mixtures of them were determined by the regular reflection (RR) photometric method combined with a thermal method. In the region of phase transitions, plateaus are observed on the heating curves of the individual waxes and steps were observed on the RR curve. In the case of mixtures of waxes, there were no plateaus on the heating curves and the steps on the RR curves persisted. The high sensitivity of the photometric method allowed determining the indicated temperatures with sufficiently high accuracy and with no plateaus on the heating curves. The RR principle on which the method is based allows investigating a wide range of objects of different natures: transparent and opaque, mixtures and dilute solutions. Rapid processing of the data and their graphic representation and archiving are possible due to automation of the method.
引用
收藏
页码:65 / 70
页数:6
相关论文
共 2 条
[1]  
BOGDANOV NF, 1961, DEWAXING PETROLEUM P
[2]  
SHISHKIN YL, 2006, KHIM TEKH TOPL MASEL, P48