Synthesis, NMR conformational studies and host-guest behaviour of new (+)-tartaric acid derivatives

被引：10
|
作者：
Legrand, S
Luukinen, H
Isaksson, R
Kilpeläinen, I
Lindström, M
Nicholls, IA
Unelius, CR [1 ]
机构：
[1] Univ Kalmar, Dept Chem & Biomed Sci, SE-39182 Kalmar, Sweden
[2] Univ Oulu, Dept Chem, FIN-90014 Oulu, Finland
[3] Univ Helsinki, Inst Biotechnol, FIN-00014 Helsinki, Finland
[4] Univ Helsinki, Dept Chem, FIN-00014 Helsinki, Finland
[5] STI Packforsk AB, SE-11486 Stockholm, Sweden
来源：
TETRAHEDRON-ASYMMETRY | 2005年 / 16卷 / 03期
关键词：
D O I：
10.1016/j.tetasy.2004.11.025
中图分类号：
O61 [无机化学];
学科分类号：
070301 ; 081704 ;
摘要：
A series of dimeric alpha,alpha,alpha',alpha'-tetraaryl-1,3-dioxolane-4,5-dimethanol TADDOLs has been prepared and host-guest interactions of these structures have been characterized using a series of H-1 NMR studies. Enantioselective recognition of the chiral alcohols glycidol and menthol was observed for phenyl and 2-naphthyl derivatives. The influence of steric bulk on the dynamic fluxional behaviour of the TADDOL structures was demonstrated by dynamic NMR. (C) 2004 Elsevier Ltd. All rights reserved.
引用
收藏
页码：635 / 640
页数：6
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