On the application of the work-of-indentation approach to depth-sensing indentation experiments in coated systems

被引:112
作者
Tuck, JR [1 ]
Korsunsky, AM [1 ]
Bull, SJ [1 ]
Davidson, RI [1 ]
机构
[1] Univ Newcastle Upon Tyne, Dept Mech Mat & Mfg Engn, Div Mat, Newcastle Upon Tyne NE1 7RU, Tyne & Wear, England
基金
英国工程与自然科学研究理事会;
关键词
characterization model; vickers hardness test; nano-indentation; atomic force microscopy (AFM); ion beam; evaporation; arc evaporation;
D O I
10.1016/S0257-8972(00)01063-X
中图分类号
TB3 [工程材料学];
学科分类号
0805 ; 080502 ;
摘要
The work-of-indentation approach is developed and applied for hardness calculations in soft or hard materials, and also for a range of coated systems. The method appears to be less sensitive than other definitions to the effects of pile-up observed in soft materials. Work-of-indentation hardness is calculated directly from the energy of indentation without the need for estimating penetration depths, areas or volumes, which can be time consuming and inaccurate. In particular, using the plastic component of the work-of-indentation yields consistent results across the range of materials studied. The method breaks down, however, at very low loads and small penetration depths, which is likely to be due to deviations from the ideal tip geometry. (C) 2001 Elsevier Science B.V. All rights reserved.
引用
收藏
页码:217 / 224
页数:8
相关论文
共 11 条
[1]   Influences of pileup on the measurement of mechanical properties by load and depth sensing indentation techniques [J].
Bolshakov, A ;
Pharr, GM .
JOURNAL OF MATERIALS RESEARCH, 1998, 13 (04) :1049-1058
[2]   Effects of 'sinking in' and 'piling up' on estimating the contact area under load in indentation [J].
Cheng, YT ;
Cheng, CM .
PHILOSOPHICAL MAGAZINE LETTERS, 1998, 78 (02) :115-120
[3]   On the hardness of coated systems [J].
Korsunsky, AM ;
McGurk, MR ;
Bull, SJ ;
Page, TF .
SURFACE & COATINGS TECHNOLOGY, 1998, 99 (1-2) :171-183
[4]   Arc evaporated Ti-N films with reduced macroparticle contamination [J].
Kourtev, J ;
Pascova, R ;
Weissmantel, E .
THIN SOLID FILMS, 1996, 287 (1-2) :202-207
[5]  
MCCABE AR, 1993, ROYAL SOC CHEM SPECI, V127, P163
[6]   AN IMPROVED TECHNIQUE FOR DETERMINING HARDNESS AND ELASTIC-MODULUS USING LOAD AND DISPLACEMENT SENSING INDENTATION EXPERIMENTS [J].
OLIVER, WC ;
PHARR, GM .
JOURNAL OF MATERIALS RESEARCH, 1992, 7 (06) :1564-1583
[7]   USING NANOINDENTATION TECHNIQUES FOR THE CHARACTERIZATION OF COATED SYSTEMS - A CRITIQUE [J].
PAGE, TF ;
HAINSWORTH, SV .
SURFACE & COATINGS TECHNOLOGY, 1993, 61 (1-3) :201-208
[8]  
PLUMB S, 1985, METALLURGIA, V52, P59
[9]   ELASTIC RECOVERY OF CONICAL INDENTATIONS [J].
STILWELL, NA ;
TABOR, D .
PROCEEDINGS OF THE PHYSICAL SOCIETY OF LONDON, 1961, 78 (500) :169-&
[10]   Influences of stress on the measurement of mechanical properties using nanoindentation .1. Experimental studies in an aluminum alloy [J].
Tsui, TY ;
Oliver, WC ;
Pharr, GM .
JOURNAL OF MATERIALS RESEARCH, 1996, 11 (03) :752-759