A versatile one-pot synthesis of dialkyl disulfides and sulfides

被引:26
|
作者
Emerson, DW [1 ]
Bennett, BL [1 ]
Steinberg, SM [1 ]
机构
[1] Univ Nevada, Dept Chem, Las Vegas, NV 89154 USA
关键词
disulfides; fluorine and fluorine compounds; sulfides;
D O I
10.1081/SCC-200050331
中图分类号
O62 [有机化学];
学科分类号
070303 ; 081704 ;
摘要
Conversions of moncifluoroalkyl and alkyl bromides to the corresponding dialkyl disulfides in a one-pot synthesis using thiourea followed by basic hydrogen peroxide are described. Modified methods afford access to unsymmetrical disulfides and sulfides.
引用
收藏
页码:631 / 638
页数:8
相关论文
共 50 条
  • [21] One-pot Metal-free Synthesis of Benzyl Alkyl Sulfides
    Lu, Xiaogang
    Wang, Hongmei
    Gao, Runli
    Pei, Chengxin
    PHOSPHORUS SULFUR AND SILICON AND THE RELATED ELEMENTS, 2015, 190 (01) : 45 - 52
  • [22] One-Pot Preparation of Arylethynyl Sulfides and Bis(arylethynyl) Sulfides
    Su, Qiong
    Zhao, Zi-Jian
    Xu, Feng
    Lou, Peng-Cai
    Zhang, Kai
    Xie, De-Xun
    Shi, Lei
    Cai, Qing-Yun
    Peng, Zhi-Hong
    An, De-Lie
    EUROPEAN JOURNAL OF ORGANIC CHEMISTRY, 2013, 2013 (08) : 1551 - 1557
  • [23] Inexpensive, one-pot synthesis of unsymmetrical disulfides using 1-chlorobenzotriazole
    Hunter, Roger
    Caira, Mino
    Stellenboom, Nashia
    JOURNAL OF ORGANIC CHEMISTRY, 2006, 71 (21): : 8268 - 8271
  • [24] A ONE-POT SYNTHESIS OF (S,S)-DIALKYL-N-(PERFLUOROALKYLSULFONYL)CARBODITHIOIMIDATES
    LI, AW
    BIN, X
    ZHU, SZ
    JOURNAL OF FLUORINE CHEMISTRY, 1994, 69 (03) : 257 - 259
  • [25] A one-pot synthesis of novel N,N-dialkyl-S-glycosylsulfenamides
    Owen, DJ
    von Itzstein, M
    CARBOHYDRATE RESEARCH, 2000, 328 (03) : 287 - 292
  • [26] A NEW ONE-POT SYNTHESIS OF DIALKYL PHOSPHONATES FROM DIAZO-COMPOUNDS AND DIALKYL HYDROGEN PHOSPHITES
    POLOZOV, AM
    POLEZHAEVA, NA
    MUSTAPHIN, AH
    KHOTINEN, AV
    ARBUZOV, BA
    SYNTHESIS-STUTTGART, 1990, (06): : 515 - 517
  • [27] Versatile one-pot synthesis of grafted-hydrogenated natural rubber
    Kookarinrat, Chanathip
    Paoprasert, Peerasak
    IRANIAN POLYMER JOURNAL, 2015, 24 (02) : 123 - 133
  • [28] Versatile one-pot synthesis of grafted-hydrogenated natural rubber
    Chanathip Kookarinrat
    Peerasak Paoprasert
    Iranian Polymer Journal, 2015, 24 : 123 - 133
  • [29] Highly efficient and versatile one-pot synthesis of substituted thienylidene compounds
    Moghaddam, Firouz Matloubi
    Boeini, Hassan Zali
    Bagheri, Mojtaba
    Rüedi, Peter
    Linden, Anthony
    Journal of Sulfur Chemistry, 2005, 26 (03) : 245 - 250
  • [30] One-pot synthesis
    Anon
    Chemical and Engineering News, 2002, 80 (46):