Volatile compounds of leaves and fruits of Mangifera indica var. coquinho (Anacardiaceae) obtained using solid phase microextraction and hydrodistillation

被引：36

作者：

Gebara, Samya Soler ^{[1
]}

Ferreira, Wellyta de Oliveira ^{[1
]}

Re-Poppi, Nilva ^{[1
]}

Simionatto, Euclesio ^{[2
]}

Carasek, Eduardo ^{[3
]}

机构：

[1] Univ Fed Mato Grosso do Sul, Dept Quim, BR-79080190 Campo Grande, MS, Brazil

[2] Univ Fed Mato Grosso do Sul, Dept Hidraul & Transporte, BR-79070900 Campo Grande, MS, Brazil

[3] Univ Fed Santa Catarina, Dept Quim, BR-88040900 Florianopolis, SC, Brazil

来源：

FOOD CHEMISTRY | 2011年 / 127卷 / 02期

关键词：

Mangifera indica var. coquinho; Essential oil composition; Solid phase microextraction; Hydrodistillation; ESSENTIAL OIL COMPOSITION; CHEMICAL-COMPOSITION; HEADSPACE; EXTRACTION; PROFILE; FIBERS; ZRO2; L;

D O I：

10.1016/j.foodchem.2010.12.123

中图分类号：

O69 [应用化学];

学科分类号：

081704 ;

摘要：

Volatile compounds present on fruits and leaves of Mangifera indica var. coquinho were investigated by headspace solid phase microextraction (HS-SPME) and hydrodistillation (HD). Conventional techniques, such as hydrodistillation, may impart chemical changes to the original oil composition being also time-consuming. On the other hand, HS-SPME provides solvent-less extractions, shorter extraction times and may supply complementary information about the composition of the compounds. The HS-SPME technique was previously evaluated by the comparative study among the fibres: commercial PDMS, NiTi-ZrO2 and NiTi-ZrO2-PDMS. The fibre NiTi-ZrO2-PDMS showed better sensitivity and precision and was used on the extraction of components. The influence of several parameters like the time and temperature of extraction and desorption time were examined to obtain better efficiency. Fruits and leaves were analysed in mature and immature stages. The profiles corresponding to the volatile compounds detected by both techniques are discussed. (C) 2011 Elsevier Ltd. All rights reserved.

引用

页码：689 / 693

页数：5

共 22 条

[1]

Adams R.P., 2004, Identification of Essential Oil Components by Gas Chromatography/Quadrupole Mass Spectroscopy

[2]

Andrade Eloisa Helena A., 2000, Journal of Food Composition and Analysis, V13, P27, DOI 10.1006/jfca.1999.0841

[3] SOLID-PHASE MICROEXTRACTION WITH THERMAL-DESORPTION USING FUSED-SILICA OPTICAL FIBERS [J].

ARTHUR, CL ;

PAWLISZYN, J .

ANALYTICAL CHEMISTRY, 1990, 62 (19) :2145-2148

[4] Development of a headspace-solid phase micro extraction method to monitor changes in volatile profile of rose (Rosa hybrida, cv David!Austin) petals during processing [J].

Bianchi, Giulia ;

Nuzzi, Monica ;

Leva, Alexa Avitabile ;

Rizzolo, Anna .

JOURNAL OF CHROMATOGRAPHY A, 2007, 1150 (1-2) :190-197

[5] Headspace sampling of the volatile fraction of vegetable matrices [J].

Bicchi, Carlo ;

Cordero, Chiara ;

Liberto, Erica ;

Sgorbini, Barbara ;

Rubiolo, Patrizia .

JOURNAL OF CHROMATOGRAPHY A, 2008, 1184 (1-2) :220-233

[6] Reliability of fibres in solid-phase microextraction for routine analysis of the headspace of aromatic and medicinal plants [J].

Bicchi, Carlo ;

Cordero, Chiara ;

Liberto, Erica ;

Sgorbini, Barbara ;

Rubiolo, Patrizia .

JOURNAL OF CHROMATOGRAPHY A, 2007, 1152 (1-2) :138-149

[7] Preparation and characterization of new solid-phase microextraction fibers obtained by sol-gel technology and zirconium oxide electrodeposited on NiTi alloy [J].

Budziak, Dilma ;

Martendal, Edmar ;

Carasek, Eduardo .

JOURNAL OF CHROMATOGRAPHY A, 2008, 1187 (1-2) :34-39

[8] Preparation and application of NiTi alloy coated with ZrO2 as a new fiber for solid-phase microextraction [J].

Budziak, Dilma ;

Martendal, Edmar ;

Carasek, Eduardo .

JOURNAL OF CHROMATOGRAPHY A, 2007, 1164 (1-2) :18-24

[9] Application of NiTi alloy coated with ZrO2 as a new fiber for solid-phase microextraction for determination of halophenols in water samples [J].

Budziak, Dilma ;

Martendal, Edmar ;

Carasek, Eduardo .

ANALYTICA CHIMICA ACTA, 2007, 598 (02) :254-260

[10] Comparison of static headspace, headspace solid phase microextraction, headspace sorptive extraction, and direct thermal desorption techniques on chemical composition of french olive oils [J].

Cavalli, JF ;

Fernandez, X ;

Lizzani-Cuvelier, L ;

Loiseau, AM .

JOURNAL OF AGRICULTURAL AND FOOD CHEMISTRY, 2003, 51 (26) :7709-7716

← 1 2 3 →