Wide-angle diamond cell for neutron scattering

被引:19
|
作者
Haberl, Bianca [1 ]
Dissanayake, Sachith [1 ]
Ye, Feng [1 ]
Daemen, Luke L. [1 ]
Cheng, Yongqiang [1 ]
Li, Chen W. [2 ]
Ramirez-Cuesta, A. -J. [1 ]
Matsuda, Masaaki [1 ]
Molaison, Jamie J. [1 ]
Boehler, Reinhard [1 ,3 ]
机构
[1] Oak Ridge Natl Lab, Neutron Sci Directorate, Neutron Scattering Div, Oak Ridge, TN 37831 USA
[2] Univ Calif Riverside, Mech Engn Mat Sci & Engn, Riverside, CA 92521 USA
[3] Carnegie Inst Sci, Geophys Lab, 5251 Broad Branch Rd NW, Washington, DC 20015 USA
关键词
High pressure neutron scattering; diamond anvil cell; inelastic neutron scattering; HIGH-PRESSURE; DIFFRACTION;
D O I
10.1080/08957959.2017.1390571
中图分类号
O4 [物理学];
学科分类号
0702 ;
摘要
A new diamond cell with extreme apertures is described. It is tailored for a large variety of neutron scattering techniques such as inelastic neutron scattering and single-crystal diffraction both at the Spallation Neutron Source (SNS) and the High Flux Isotope Reactor at the Oak Ridge National Laboratory. Simple springs enable forces of over 10 metric tons to be clamped in for low-temperature measurements. At present, low-cost polycrystalline diamond (Versimax((R))) pressure anvils are used. We predict a routine pressure regime up to 20GPa with sample volumes of approximate to 0.5mm(3). Future use of large CVD single-crystal diamond anvils will significantly expand this pressure range. We show examples for measurements at the SNAP, VISION and CORELLI beamlines of the SNS.
引用
收藏
页码:495 / 506
页数:12
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