THERMAL TREATMENT OF KAOLIN CLAY TO OBTAIN METAKAOLIN

被引:189
作者
Ilic, Biljana R. [1 ]
Mitrovic, Aleksandra A. [1 ]
Milicic, Ljiljana R. [1 ]
机构
[1] Inst Testing Mat, Belgrade, Serbia
关键词
Kaolin; Metakaolin; Calcination; Dehydroxylation; POZZOLANIC ACTIVITY; CEMENT PASTES; HYDRATION; CONCRETE;
D O I
10.2298/HEM1N01003220141
中图分类号
TQ [化学工业];
学科分类号
0817 ;
摘要
The metakaolin was produced by thermal treatment (calcination) of the starting high-quality kaolin clay from Serbia. The optimal calcination parameters, for which nearly complete dehydroxylation of the material was achieved, are: temperature 650 degrees C and heating time of 90 min. The conversion of the kaolinite to metakaolinite was confirmed by XRD and IR analyses of the starting and thermally treated kaolin samples. The pozzolanic activity was determined by Chapelle test. The obtained value 0.65 g Ca(OH)(2)/g of metakaolin indicates that produced metakaolin may be used as supplementary cementitious material.
引用
收藏
页码:351 / 356
页数:6
相关论文
共 21 条
[1]  
[Anonymous], Mineralogy Database
[2]   Properties of blended cements with thermally activated kaolin [J].
Arikan, Metin ;
Sobolev, Konstantin ;
Ertuen, Tomris ;
Yeginobali, Asim ;
Turker, Pelin .
CONSTRUCTION AND BUILDING MATERIALS, 2009, 23 (01) :62-70
[3]   Metakaolin as supplementary cementitious material - Optimization of kaolin to metakaolin conversion [J].
Badogiannis, E ;
Kakali, G ;
Tsivilis, S .
JOURNAL OF THERMAL ANALYSIS AND CALORIMETRY, 2005, 81 (02) :457-462
[4]   Mechanism of hydration of the metakaolin-lime-water system [J].
Cabrera, J ;
Rojas, MF .
CEMENT AND CONCRETE RESEARCH, 2001, 31 (02) :177-182
[5]   Pore size distribution and degree of hydration of metakaolin-cement pastes [J].
Frías, M ;
Cabrera, J .
CEMENT AND CONCRETE RESEARCH, 2000, 30 (04) :561-569
[6]  
ILIC B, 2010, 3 INT NAUCN STRUCN S, P711
[7]   Thermal treatment of kaolin: the effect of mineralogy on the pozzolanic activity [J].
Kakali, G ;
Perraki, T ;
Tsivilis, S ;
Badogiannis, E .
APPLIED CLAY SCIENCE, 2001, 20 (1-2) :73-80
[8]  
Kostuch J A., 1996, Concrete 2000: economic and durable const ruction through excellence, E, P1799
[9]  
KOSTUCH JA, 1993, CONCRETE 2000, V2, P1799
[10]  
Largent R., 1978, B LIAISON LAB PONT C, P61