GREEN SYNTHESIS OF SYMMETRICAL CARBONATE FT-IR STUDY

被引：2

作者：

Segneanu, Adina-Elena ^{[1
]}

Pop, Raluca ^{[1
]}

Balcu, Ione ^{[1
]}

Macarie, Corina ^{[1
]}

Milea, Marius ^{[2
]}

Martagiu, Raluca ^{[1
]}

Vaszilcsin, Cristian George ^{[1
]}

机构：

[1] Natl Inst R&D Electrochem & Condensed Matter INCE, Timisoara 300569, Romania

[2] Univ Politehn Timisoara, Fac Ind Chem & Environm Engn, Timisoara 300006, Romania

来源：

ENVIRONMENTAL ENGINEERING AND MANAGEMENT JOURNAL | 2010年 / 9卷 / 08期

关键词：

endo-N-hydroxi-5-norbomen-2,3-dicarboximide; symmetrical reactive carbonates;

D O I：

10.30638/eemj.2010.147

中图分类号：

X [环境科学、安全科学];

学科分类号：

08 ; 0830 ;

摘要：

An original method for the preparation of N,N'-bis(endo-5-norbornen-2,3-dicarboxy-imidyl) carbonate from endo-N-hydroxy-5-norbomen-2,3-dicarboximide in basic catalyst has been investigated. FT-IR studies performed in order to monitor the reaction allowed the identifying of the laboratory optimal conditions (reaction time, molar ratio). The method requires limited quantities of organic solvents and reagents, leading to an economical and environmental friendly process for the preparation of a new symmetrical organic carbonate.

引用

页码：1139 / 1143

页数：5

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