Synthesis and X-ray crystal structures of novel oxathiadibenzocrown ethers

被引：19
作者：
Lee, YH
Lee, SS [1 ]
机构：
[1] Gyeongsang Natl Univ, Dept Chem, Chinju 660701, South Korea
[2] Gyeongsang Natl Univ, Res Inst Nat Sci, Chinju 660701, South Korea
来源：
JOURNAL OF INCLUSION PHENOMENA AND MACROCYCLIC CHEMISTRY | 2001年 / 39卷 / 3-4期
基金：
新加坡国家研究基金会;
关键词：
oxathia macrocycles; synthesis; cyclization; X-ray crystalstructures;
D O I：
10.1023/A:1011116404850
中图分类号：
O6 [化学];
学科分类号：
0703 ;
摘要：
The novel 1,12-dithia macrocycles based on dibenzo substituents, 5 (S2O3), 6 (S3O2) and 7 (S2O4) have been synthesized by cesium carbonate promoted ring closure reactions of 2,2'-(ethylenedioxy)bis(benzyl chloride), 3, with the appropriate dithiols under high dilution condition in reasonable yields. The structures of macrocycles 6 and 7 have been characterized by X-ray crystallography.
引用
收藏
页码：235 / 239
页数：5
相关论文
共 50 条
  • [41] The Synthesis, X-ray Crystal Structure and Optical Properties of Novel 5-aryl-3-ferrocenyl-1-pyridazinyl-pyrazoline Derivatives
    Gong, Zhong-Liang
    Xie, Yong-Sheng
    Zhao, Bao-Xiang
    Lv, Hong-Shui
    Liu, Wei-Yong
    Zheng, Liang-Wen
    Lian, Song
    JOURNAL OF FLUORESCENCE, 2011, 21 (01) : 355 - 364
  • [42] Synthesis and X-ray crystal structure of 1,2-diaminepropane platinum(II) cantharidinate
    Wang, YH
    Huang, ZX
    Wu, C
    POLYHEDRON, 1997, 16 (01) : 57 - 59
  • [43] The synthesis, optical properties and x-ray crystal structure of novel 1,3,4-oxadiazole derivatives carrying a thiophene unit
    Li, Hailin
    Kang, Sishun
    Xing, Zhitao
    Zeng, Haisu
    Wang, Haibo
    DYES AND PIGMENTS, 2009, 80 (01) : 163 - 167
  • [44] Novel liquid crystal aldoximes and aldoxime ethers: Synthesis, characterization and liquid crystal behavior
    Alici, Onder
    Karatas, Ibrahim
    JOURNAL OF MOLECULAR LIQUIDS, 2016, 221 : 1243 - 1248
  • [45] Synthesis, X-ray crystal structure and optical properties research of novel diphenyl sulfone-based bis-pyrazoline derivatives
    Gong, Zhong-Liang
    Zheng, Liang-Wen
    Zhao, Bao-Xiang
    JOURNAL OF LUMINESCENCE, 2012, 132 (02) : 318 - 324
  • [46] Exclusive Solvent-Controlled Regioselective Catalytic Synthesis of Potentially Bioactive Imidazolidineiminodithiones: NMR Analysis, Computational Studies and X-ray Crystal Structures
    Moussa, Ziad
    Saada, Sara
    Paz, Alejandro Perez
    Alzamly, Ahmed
    Judeh, Zaher M. A.
    Alshehhi, Aaesha R.
    Khudhair, Aisha
    Almheiri, Salama A.
    Al-Masri, Harbi Tomah
    Ahmed, Saleh A.
    MOLECULES, 2024, 29 (16):
  • [47] Synthesis and structural study of precursors of novel methylsilanediols by IR and Raman spectroscopies, single-crystal X-ray diffraction and DFT calculations
    Rodriguez Ortega, M. P. G.
    Docampo, M. L.
    Thomas, L. H.
    Montejo, M.
    Marchal Ingrain, A.
    Wilson, C. C.
    Lopez Gonzalez, J. J.
    SPECTROCHIMICA ACTA PART A-MOLECULAR AND BIOMOLECULAR SPECTROSCOPY, 2014, 118 : 828 - 834
  • [48] The complex approach to the synthesis of [W(CN)6(bpy)]2-/- ion complexes. The X-ray crystal structures of reaction products
    Szklarzewicz, Janusz
    Hodorowicz, Maciej
    Jurowska, Anna
    INORGANICA CHIMICA ACTA, 2023, 546
  • [49] Molecular structures of two copper complexes with the pharmaceuticals norfloxacin and tinidazole, when powder X-ray distraction assists multi-domain single-crystal X-ray diffraction
    Tobon Zapata, Gloria Elena
    Martinez Carmona, Dina Marcela
    Alberto Echeverria, Gustavo
    Enrique Piro, Oscar
    ACTA CRYSTALLOGRAPHICA SECTION B-STRUCTURAL SCIENCE CRYSTAL ENGINEERING AND MATERIALS, 2022, 78 : 490 - 498
  • [50] SYNTHESIS, X-RAY CRYSTAL STRUCTURE, AND COMPUTATIONAL STUDY OF NOVEL PYRAZOLO[3,4-B]PYRIDIN-3-Ol DERIVATIVES
    Shen, Li-Qun
    Tang, Yong
    Wu, Ai-Qun
    Pan, Dan
    Diao, Kai-Sheng
    PHOSPHORUS SULFUR AND SILICON AND THE RELATED ELEMENTS, 2014, 189 (05) : 674 - 686
12345