Reaction of 6-arylidene-2,2-dimethylcyclohexanones with phenylhydrazine. Molecular and crystal structures of 3-(4-halopheny1)-1-pheny1-4,5,6,7-tetrahydro-(2H)-indazoles

被引：2

作者：

Gar, M. M. ^{[1
]}

Eremeev, A. V. ^{[1
]}

Suponitsky, K. Yu. ^{[2
]}

Popkov, S. V. ^{[1
]}

机构：

[1] DI Mendeleev Univ Chem Technol Russia, Moscow 125047, Russia

[2] Russian Acad Sci, AN Nesmeyanov Organoelement Cpds Inst, Moscow 119991, Russia

来源：

RUSSIAN CHEMICAL BULLETIN | 2014年 / 63卷 / 05期

关键词：

6-arylidene-2,2-dimethylcyclohexanones; 3-aryl-7; 7-dimethy1-2-phenyl-3,3a,4,5,6,7-hexahydroindazoles; 3-aryl-7,7-dimethy1-2-phenyl-4,5,6,7-tetrahydroindazoles; X-ray diffraction study; phenylhydrazine; cyclocondensation; DERIVATIVES; INHIBITORS;

D O I：

10.1007/s11172-014-0562-2

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

The previously unknown 3-(4-chloropheny1)-7,7-dimethy1-2-pheny1-3,3a,4,5,6,7-hexahydroindazole 6a and (4-halopheny1)-7,7-dimethy1-1-phenyl-4,5,6,7-tetrahydroindazoles 7a,b were synthesized by the reaction of 6-arylidene-2,2-dimethylcyclohexanones with phenylhydrazine in the presence of pyridine. The molecular and crystal structures of compounds 7a,b were determined by X-ray diffraction.

引用

页码：1142 / 1147

页数：6

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