Reconstructing intragranular strain fields in polycrystalline materials from scanning 3DXRD data

被引:44
作者
Henningsson, N. Axel [1 ]
Hall, Stephen A. [1 ]
Wright, Jonathan P. [2 ]
Hektor, Johan [3 ,4 ]
机构
[1] Lund Univ, Div Solid Mech, Box 118, S-22100 Lund, Sweden
[2] European Synchrotron Radiat Facil, 71 Ave Martyrs, F-38000 Grenoble, France
[3] DESY, Notkestr 85, D-22607 Hamburg, Germany
[4] Helmholtz Zentrum Geesthacht, Notkestr 85, D-22607 Hamburg, Germany
关键词
intragranular strain; X-ray diffraction; 3DXRD; tomography; X-RAY; GRAIN-BOUNDARIES; ALGORITHM; MAPS;
D O I
10.1107/S1600576720001016
中图分类号
O6 [化学];
学科分类号
0703 ;
摘要
Two methods for reconstructing intragranular strain fields are developed for scanning three-dimensional X-ray diffraction (3DXRD). The methods are compared with a third approach where voxels are reconstructed independently of their neighbours [Hayashi, Setoyama & Seno (2017). Mater. Sci. Forum, 905, 157-164]. The 3D strain field of a tin grain, located within a sample of approximately 70 grains, is analysed and compared across reconstruction methods. Implicit assumptions of sub-problem independence, made in the independent voxel reconstruction method, are demonstrated to introduce bias and reduce reconstruction accuracy. It is verified that the two proposed methods remedy these problems by taking the spatial properties of the inverse problem into account. Improvements in reconstruction quality achieved by the two proposed methods are further supported by reconstructions using synthetic diffraction data.
引用
收藏
页码:314 / 325
页数:12
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