High-Performance Adsorption of 4-Nitrophenol onto Calix[6]arene-Tethered Silica from Aqueous Solutions

被引：27

作者：

Dogan, Murat ^{[1
]}

Temel, Farabi ^{[2
]}

Tabakci, Mustafa ^{[2
]}

机构：

[1] Necmettin Erbakan Univ, Grad Sch Nat & Appl Sci, Konya 42140, Turkey

[2] Konya Tech Univ, Dept Chem Engn, Konya 42130, Turkey

来源：

JOURNAL OF INORGANIC AND ORGANOMETALLIC POLYMERS AND MATERIALS | 2020年 / 30卷 / 10期

关键词：

Phenol removal; Organic pollutants; Adsorption; Calixarene; Silica support; COATED QCM SENSORS; P-NITROPHENOL; PHENOLIC-COMPOUNDS; GEL; SORPTION; REMOVAL; POLYMER; IMMOBILIZATION; EQUILIBRIUM; OXIDATION;

D O I：

10.1007/s10904-020-01571-0

中图分类号：

O63 [高分子化学（高聚物）];

学科分类号：

070305 ; 080501 ; 081704 ;

摘要：

The polymeric calix[6]arene-tethered silica (C[6]TS) was prepared by the tethering of p-tert-butylcalix[6]arene onto 3-glycidoxypropyl-bonded stationary phase. The structural and composition analysis of the C[6]TS was performed by FTIR, XRD, TGA, and SEM techniques. C[6]TS was used as an adsorbent for the removal of 4-nitrophenol (4-NP) from aqueous solutions. Initial adsorption experiments demonstrated that C[6]TS showed outstanding performance for the removal of 4-NP. So it exhibited rapid and effective adsorption with a %83 yield within ten minutes. Subsequently, some adsorption criteria such as pH, initial concentration, contact time, sorbent dosage, and temperature were evaluated in detail. Thus, adsorption phenomena of 4-NP onto C[6]TS were clarified in this way.

引用

页码：4191 / 4202

页数：12

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