Study of deterioration of historical parchments by various thermal analysis techniques complemented by SEM, FTIR, UV-Vis-NIR and unilateral NMR investigations

被引：107

作者：

Badea, Elena ^{[1
]}

Miu, Lucretia ^{[2
]}

Budrugeac, P. ^{[3
]}

Giurginca, Maria ^{[4
]}

Masic, A. ^{[1
]}

Badea, Nicoleta ^{[4
]}

Della Gatta, G. ^{[1
]}

机构：

[1] Univ Turin, IFM, Dept Chem, I-10125 Turin, Italy

[2] Natl Res & Dev Inst Text & Leather, Bucharest 031215, Romania

[3] Natl Inst Res & Dev Elect Engn ICPE CA, Bucharest 030138, Romania

[4] Univ Politehn Bucuresti, Bucharest 011061, Romania

来源：

JOURNAL OF THERMAL ANALYSIS AND CALORIMETRY | 2008年 / 91卷 / 01期

关键词：

deterioration pathways; DSC; DTA; FTIR; historical parchments; NMR; SEM; TG; thermal analysis; UV-Vis-NIR;

D O I：

10.1007/s10973-007-8513-x

中图分类号：

O414.1 [热力学];

学科分类号：

摘要：

A comprehensive investigation has been made of a set of 14(th) to 16(th)-century parchment bookbindings from the Historical Archives of the City of Turin. Advanced physico-chemical techniques, such as thermal analysis (DSC, TG and DTA), spectroscopy (FTIR and UV-Vis-NIR), scanning electron microscopy (SEM) and unilateral nuclear magnetic resonance (NMR-ProFiler) were employed to assess specific deterioration processes occurring at different levels in the hierarchical structure of parchment. Changes in the measured physical and chemical parameter values of parchment due to interaction with the environment were used to identify possible deterioration pathways.

引用

页码：17 / 27

页数：11

共 51 条

[1] Solid-state NMR studies of collagen-based parchments and gelatin [J].