Synthesis and Characterization of Ni(II) Schiff Base Macrocyclic Complexes

被引：0
作者：
Golbedaghi, Reza [1 ]
机构：
[1] Payame Noor Univ, Dept Chem, Tehran 193954697, Iran
来源：
ASIAN JOURNAL OF CHEMISTRY | 2011年 / 23卷 / 09期
关键词：
Cyclocondensation; Tripodal; Macrocyclic complex; METAL-COMPLEXES; LIGANDS; COPPER;
D O I：
暂无
中图分类号：
O6 [化学];
学科分类号：
0703 ;
摘要：
[2+2]Cyclocondensation of L(22py) = N-(2-pyridylmethyl)-N-(2-aminoethyl)-1,2-diaminoethane, L(23py) = N-(2-pyridylmethyl)-N-(2-aminoethyl)-1,3-diaminopropane and 2-[3-(2-formyl phenoxy)propoxy]benzaldehye and 2-[4-(2-formyl phenoxy)butoxy]benzaldehyde in the presence of Ni(ClO(4))(2)center dot 4H(2)O in equimolar ratios gave three new binuclear Ni(II) macrocyclic complexes. Resulting compounds, [{Ni(H(2)L(1))](ClO(4))(2) (1), [Ni(H(2)L(2))](ClO(4))(2) (2) and [Ni(H(2)L(3))](ClO(4))(2) (3), were characterized by IR spectroscopy and elemental analysis. The Ni(II) ions in latter complexes are six coordinated.
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收藏
页码：4239 / 4240
页数：2
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