Synthesis and spectroscopic [IR, NMR (1H, 13C, 29Si)] characterization of methylsilyl N-arylsalicylaldiminates

被引：12

作者：

Goyal, M ^{[1
]}

Mishra, S ^{[1
]}

Singh, A ^{[1
]}

机构：

[1] Univ Rajasthan, Dept Chem, Jaipur 302004, Rajasthan, India

来源：

PHOSPHORUS SULFUR AND SILICON AND THE RELATED ELEMENTS | 2001年 / 175卷

关键词：

methylsilyl compounds; Schiff base complexes; N-arylsalicylaldiminates;

D O I：

10.1080/10426500108040262

中图分类号：

O61 [无机化学];

学科分类号：

070301 ; 081704 ;

摘要：

Reactions of MeSiCl3 in 1:1, 1:2, and 1:3 molar ratios with HOC6H4CH=NAr (Ar = C6H3Me2-2,6; C6H2Me3-2,4,6; and C6H3Et2-2,6) in the presence of Et3N or C5H5N as a base afford compounds of the type MeSiCl3-x(OC6H4CH=NAr)(x) (x = 1, 2, and 3). Characterization of all these species have been carried out by elemental analysis, molecular weight determinations, and spectroscopic [IR, NMR (H-1, C-13 and Si-29)] studies.

引用

页码：143 / 152

页数：10

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