Structural and Morphological Studies under Small-Angle Neutron Scattering of Tungsten Alloys

被引:13
作者
Demir, Ertugrul [1 ,2 ]
Gledenov, Yury M. [2 ]
Tugrul, A. Beril [1 ]
Mirzayev, Matlab N. [2 ,3 ]
Islamov, Ahmed Kh. [2 ]
Turchenko, Vitaly A. [2 ]
Yilmaz, Ozan [1 ]
Buyuk, Bulent [4 ]
Sansarbayar, Enkhbold [2 ]
Ovecoglu, M. Lutfi [1 ]
机构
[1] Istanbul Tech Univ, Energy Inst, TR-34469 Istanbul, Turkey
[2] Joint Inst Nucl Res, Moscow 141980, Russia
[3] Azerbaijan Natl Acad Sci, Inst Radiat Problems, AZ-1143 Baku, Azerbaijan
[4] Bandirma Onyedi Eylul Univ, TR-10200 Bandirma, Balikesir, Turkey
关键词
tungsten composites; Raman spectroscopy; small-angle neutron scattering; X-ray diffraction; mechanical alloying; BORON-CARBIDE; MICROSTRUCTURE; EVOLUTION; STATE;
D O I
10.3103/S0027134919050059
中图分类号
O4 [物理学];
学科分类号
0702 ;
摘要
In the present work, tungsten composites were mechanically alloyed for 6 h and sintered at 1750 degrees C under N-2, H-2 gas flowing conditions. Phase and microstructural characterization investigations of tungsten alloys were carried out using X-ray diffraction, scanning electron microscopy, small-angle neutron scattering, and Raman spectroscopy. Tungsten boron and tungsten boride as major phases were determined in the X-ray diffraction patterns. Raman spectra indicated the existence of the carbon phases, which are the disordered graphite (D) and graphite (C). Small-angle neutron scattering measurements were performed to obtain the distribution of powders. The results were in good agreement with scanning electron microscopy findings.
引用
收藏
页码:509 / 513
页数:5
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