Star-shaped PbS nanocrystals prepared by hydrothermal process in the presence of thioglycolic acid

被引：131
作者：
Salavati-Niasari, Masoud [1 ]
Ghanbari, Davood [2 ]
Loghman-Estarki, Mohammad Reza [3 ]
机构：
[1] Univ Kashan, Inst Nano Sci & Nano Technol, Kashan, Iran
[2] Islamic Azad Univ, Arak Branch, Arak, Iran
[3] Isfahan Univ Technol, Dept Mat Engn, Esfahan, Iran
来源：
POLYHEDRON | 2012年 / 35卷 / 01期
基金：
美国国家科学基金会;
关键词：
Lead sulfide; Nanostructures; Hydrothermal; Optical properties; QUANTUM DOTS; CRYSTALS; NANOSTRUCTURES; NANOPARTICLES; GROWTH; EVOLUTION; NANORODS; ENERGY;
D O I：
10.1016/j.poly.2012.01.010
中图分类号：
O61 [无机化学];
学科分类号：
070301 ; 081704 ;
摘要：
Nanocrystalline PbS with different morphologies and particle sizes was obtained via a simple hydrothermal reaction between Pb(NO3)(2) and thioglycolic acid (TGA) at relatively low temperature. Products were characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM), transmission electron microscopy (TEM), ultraviolet-visible (UV-Vis) spectroscopy, photoluminescence (PL) and Fourier transform infrared (FT-IR) spectroscopy. Depending on the reactant concentration and molar ratio of TGA to the lead nitrate, the morphologies of the PbS crystals varied and the crystals with shapes of nanoparticles, star-like dendrite and nanorods were obtained. The effect of reaction temperature and reaction time on the morphology and particle sizes of nanocrystalline PbS products has been investigated. (C) 2012 Elsevier Ltd. All rights reserved.
引用
收藏
页码：149 / 153
页数：5
相关论文
共 37 条
  • [11] Synthesis of tetrapod like PbS microcrystals by hydrothermal route and its optical characterization
    Jana, S.
    Goswami, S.
    Nandy, S.
    Chattopadhyay, K. K.
    [J]. JOURNAL OF ALLOYS AND COMPOUNDS, 2009, 481 (1-2) : 806 - 810
  • [12] Star-shaped PbS crystals fabricated by a novel hydrothermal method
    Ji, YJ
    Ma, XY
    Zhang, H
    Xu, J
    Yang, D
    [J]. JOURNAL OF PHYSICS-CONDENSED MATTER, 2003, 15 (44) : 7611 - 7615
  • [13] Surfactant-assisted growth of novel PbS dendritic nanostructures via facile hydrothermal process
    Kuang, DB
    Xu, AW
    Fang, YP
    Liu, HQ
    Frommen, C
    Fenske, D
    [J]. ADVANCED MATERIALS, 2003, 15 (20) : 1747 - +
  • [14] Multi-level assemblies of lead sulphide nanorods
    Lu, Qingyi
    Gao, Feng
    Komarneni, Sridhar
    [J]. NANOTECHNOLOGY, 2006, 17 (10) : 2574 - 2580
  • [15] Hierarchical, star-shaped PbS crystals formed by a simple solution route
    Ma, YR
    Qi, LM
    Ma, JM
    Cheng, HM
    [J]. CRYSTAL GROWTH & DESIGN, 2004, 4 (02) : 351 - 354
  • [16] Mayers B, 2001, ADV MATER, V13, P1380, DOI 10.1002/1521-4095(200109)13:18<1380::AID-ADMA1380>3.0.CO
  • [17] 2-W
  • [18] A laser ablation method for the synthesis of crystalline semiconductor nanowires
    Morales, AM
    Lieber, CM
    [J]. SCIENCE, 1998, 279 (5348) : 208 - 211
  • [19] Nanda KK, 2001, NANO LETT, V1, P605, DOI [10.1021/nl0100318, 10.1021/n10100318]
  • [20] Shape controllable preparation of PbS crystals by a simple aqueous phase route
    Ni, YH
    Liu, HJ
    Wang, F
    Liang, YY
    Hong, JM
    Ma, X
    Xu, Z
    [J]. CRYSTAL GROWTH & DESIGN, 2004, 4 (04) : 759 - 764
1234