A facile route for large-scale synthesis of molybdenum phosphide nanoparticles with high surface area

被引：5

作者：

Song, Tingting ^{[1
]}

Shi, Yan ^{[1
]}

Yao, Zhiwei ^{[1
]}

Gao, Haifeng ^{[1
]}

Liang, Feixue ^{[1
]}

Jiang, Baojiang ^{[2
]}

Sun, Yue ^{[1
]}

Kong, Lingchao ^{[3
]}

机构：

[1] Liaoning Shihua Univ, Coll Chem Chem Engn & Environm Engn, Fushun 113001, Peoples R China

[2] Heilongjiang Univ, Minist Educ Peoples Republ China, Key Lab Funct Inorgan Mat Chem, Harbin 150080, Heilongjiang, Peoples R China

[3] Liaoning Shihua Univ, Fushun, Peoples R China

来源：

PHOSPHORUS SULFUR AND SILICON AND THE RELATED ELEMENTS | 2017年 / 192卷 / 11期

基金：

中国国家自然科学基金;

关键词：

MoP nanoparticles; large-scale synthesis; solid mixture precursor; phenol-formaldehyde resin; TRANSITION-METAL PHOSPHIDES; HYDROGEN EVOLUTION REACTION; NICKEL PHOSPHIDE; HYDRAZINE DECOMPOSITION; CONTROLLABLE SYNTHESIS; ASSISTED SYNTHESIS; CATALYSTS; ELECTROCATALYST; HYDRODESULFURIZATION; NANOSTRUCTURES;

D O I：

10.1080/10426507.2017.1330829

中图分类号：

O61 [无机化学];

学科分类号：

070301 ; 081704 ;

摘要：

In this study, we report a novel, simple and large-scale (about 100 g) synthesis of MoP nanoparticles with a high surface area (439.3m(2) g(-1)). The current approach uses a solid mixture of MoO3, (NH4)(2)HPO4 and phenol-formaldehyde resin (PFR) as a precursor and employs an inert gas as a feed gas. The formation mechanism of MoP was proposed by various techniques, including thermogravimetry-mass spectrometry (TG-MS), X-ray diffraction (XRD), X-ray photoelectron spectroscopy (XPS), and carbon content analysis.

引用

页码：1159 / 1164

页数：6

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