Data on the derived mesoporous based catalyst for the synthesized of fatty acid methyl ester (FAME) from ternary oil blend: An optimization approach

被引:8
作者
Adepoju, T. F. [1 ]
Ibeh, M. A. [1 ]
Ekanem, U. [1 ]
Asuquo, A. J. [1 ]
机构
[1] Akwa Ibom State Univ, Chem Petrochem Engn Dept, Ikot Akpaden Mkpat Enin LGA, PMB 1167, Uyo, Akwa Ibom State, Nigeria
来源
DATA IN BRIEF | 2020年 / 30卷
关键词
FAME; Citrullus lanatus; Musa acuminate; Calcination; Cucurbita pepo; Optimization; BIODIESEL PRODUCTION;
D O I
10.1016/j.dib.2020.105514
中图分类号
O [数理科学和化学]; P [天文学、地球科学]; Q [生物科学]; N [自然科学总论];
学科分类号
07 ; 0710 ; 09 ;
摘要
This work presents datasets on fatty acid methyl ester (FAME) synthesized from the ternary blend of Cucurbita pepo-chrysophyllum albidum-papaya mix oils via methanolysis of mesoporous CaO heterogeneous catalyst derived from the mixture of Citrullus lanatus and Musa acuminate peels. The oils were extracted from the milled powdered using the solvent extraction method. Ternary oil mixed ratio of 33:33:34 with low acid value and density was achieved using simplex lattice design software. Characterization of the mixed calcined catalyst powder (MCCP) at 700 degrees C for 4 h was carried out using scanning electron microscopy (SEM), energy dispersive spectroscope (EDS), X-ray diffraction analysis (XRD), and BET analysis. The thermal decomposition of mixed calcined catalyst powder (MCCP) produced 78.74% CaO with a strong basic site of 143 (mu mole.g(-1)). Fatty acid methyl ester (FAME) was synthesized through the based catalyst transesterification of a derived catalyst by considering four variables data (reaction time, reaction temperature, catalyst amount and methanol/oil molar ratio) using response surface methodology (RSM). The maximum experimental FAME data of 94.29 (wt. %) was achieved at run 16, but the central composite design (CCD) software predicted value of 98.00 (wt. %) at a reaction time of 70 min, reaction temperature of 80 degrees C, catalyst amount of 5.0 (wt.) and methanol to oil molar ratio (MeOH/OMR) of 6.97, at the desirability of 97.90%. This was validated in triplicate, and the average FAME data obtained was 93.45 (wt. %). The produced FAME properties dataset meets the standard recommended value of ASTM and EN14214. (C) 2020 The Author(s). Published by Elsevier Inc.
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页数:13
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