Preparation of columbite MgNb2O6 and ZnNb2O6 ceramics by reaction-sintering

被引:34
作者
Liou, Yi-Cheng [1 ]
Sung, Yueh-Lun [1 ]
机构
[1] Kun Shan Univ, Dept Elect Engn, Tainan 71003, Taiwan
关键词
MgNb2O6; ZnNb2O6; reaction-sintering process;
D O I
10.1016/j.ceramint.2006.10.016
中图分类号
TQ174 [陶瓷工业]; TB3 [工程材料学];
学科分类号
0805 ; 080502 ;
摘要
Columbite MgNb2O6 (MN) and ZnNb2O6 (ZN) ceramics produced by the reaction-sintering process were investigated. Secondary phases Mg0.652Nb0.598O2.25 and Mg0.66Nb11.33O29 were found in MgNb2O6 pellets. After 1250 degrees C sintering for 2 h, a density 4.85 g/cm(3) (97.1% of the theoretical value) was obtained in MgNb2O6 pellets. In ZnNb2O6 pellets, no secondary phase formed. The maximum density 5.55 g/cm(3) (98.7% of the theoretical value) occurs at 1200 and 1180 degrees C sintering for 2 and 4 h, respectively. (c) 2006 Elsevier Ltd and Techna Group S.r.l. All rights reserved.
引用
收藏
页码:371 / 377
页数:7
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