Determination of the stereochemistry of the N,N-dimethyl amino acid and the alpha-amino acid residue of peptide alkaloids by chiral gas chromatography

被引：0

作者：

daSilva, UF

Cardoso, CD

Zanatta, N

Morel, AF

Icheln, D

Gehrcke, B

机构：

[1] UNIV FED SANTA MARIA,DEPT QUIM,BR-97119900 SANTA MARIA,RS,BRAZIL

[2] UNIV HAMBURG,INST ORGAN CHEM,D-20146 HAMBURG,GERMANY

来源：

PHYTOCHEMICAL ANALYSIS | 1996年 / 7卷 / 01期

关键词：

alkaloids; stereochemistry; cyclodextrins; enantioselective gas chromatography;

D O I：

10.1002/(SICI)1099-1565(199601)7:1<20::AID-PCA285>3.0.CO;2-J

中图分类号：

Q5 [生物化学];

学科分类号：

071010 ; 081704 ;

摘要：

The stereochemistry of both the N,N-dimethyl amino acid and alpha-amino acid residues, after hydrolysis of the peptide alkaloids scutianine-B, -C, -D and -E, franganine and adoutine-Y' have been determined by gas chromatography employing modified cyclodextrins as chiral stationary phases.

引用

页码：20 / 23

页数：4

共 4 条

[1] Imaging Peptide and Protein Chirality via Amino Acid Analysis by Chiral x Chiral Two-Dimensional Correlation Liquid Chromatography
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ANALYTICAL CHEMISTRY, 2018, 90 (13) : 7963 - 7971
[2] Unusual N-pyridinium amino acid-type alkaloids from roots and rhizomes of Sophora tonkinensis Gagnep
Li, Xin
Zhang, Ning
Yang, Sheng-Li
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Zhou, Xiao-Jiao
Tian, Jin-Ying
Ye, Fei
Wang, Su-Juan
FITOTERAPIA, 2023, 165
[3] N-(N-BUTYLAMIDE) OF (S)-2-(PHENYLCARBAMOYLOXY)PROPIONIC ACID - A NEW CHIRAL SOLVATING AGENT, DERIVED FROM L-LACTIC ACID, FOR THE ENANTIOMERIC PURITY DETERMINATION OF DERIVATIZED AMINO-ACIDS
PINI, D
UCCELLOBARRETTA, G
ROSINI, C
SALVADORI, P
CHIRALITY, 1991, 3 (03) : 174 - 176
[4] Chiral metal complexes .49. Structural studies of ternary Co(II) complexes of N,N'-di(2S-pyrrolidin-2-yl)-1S,2S-diaminocyclohexane and alpha-amino acids
Cox, MA
Stephens, FS
Vagg, RS
Williams, PA
JOURNAL OF COORDINATION CHEMISTRY, 1997, 41 (04) : 275 - 290

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