Quality control of natural resins used in historical European lacquer reconstructions with some reflections on the composition of sandarac resin (Tetraclinis articulata (Vahl) Mast.)

被引:2
作者
Decq, Louise [1 ,2 ]
Stoffelen, Piet [3 ]
Cattersel, Vincent [4 ]
Mazurek, Joy [5 ]
Fremout, Wim [1 ]
Veenhoven, Jonas [1 ,2 ,6 ]
Lynen, Frederic [2 ]
Saverwyns, Steven [1 ]
Vandenabeele, Peter [2 ]
机构
[1] Royal Inst Cultural Heritage KIK IRPA, Dept Labs, Jubelpk 1, B-1000 Brussels, Belgium
[2] Univ Ghent, Dept Organ Chem, Krijgslaan 281, B-9000 Ghent, Belgium
[3] Meise Bot Garden, Nieuwelaan 38, B-1860 Meise, Belgium
[4] Univ Antwerp, Fac Design Sci, ARCHES Res Grp, Mutsaardstr 31, B-2000 Antwerp, Belgium
[5] Getty Conservat Inst, 1200 Getty Ctr Dr,Suite 700, Los Angeles, CA 90049 USA
[6] Univ Amsterdam, Fac Humanities, Amsterdam Sch Heritage Memory & Mat Culture AHM, Conservat & Restorat Cultural Heritage, POB 94552, NL-1090 GN Amsterdam, Netherlands
关键词
European lacquer; THM-GC; MS; THM-py-GC; Quality control; Resins; Sandarac; Cupressaceae; Pyrolysis; CHEMICAL-COMPOSITION; VARNISHES; SPECTROMETRY; DITERPENOIDS; COLLECTION; MIDDLE; GC/MS; ACIDS;
D O I
10.1016/j.jaap.2021.105159
中图分类号
O65 [分析化学];
学科分类号
070302 ; 081704 ;
摘要
In order to verify correct labeling and purity of natural lacquer ingredients sold today, 66 resins, gums and oils were analyzed by THM-GC/MS and compared with non-commercial reference samples. 21 deviations were found, indicating an adulteration or mislabeling of a resin. Many of the deviations occurred in sandarac resin, traditionally harvested from Tetraclinis articulata (Vahl) Mast., which seems to have another composition today than historically. Differences between both types were persistent through artificial aging. This study comprised one freshly harvested sandarac resin, as well as several specimens of historical collections, as reference material for Tetraclinis articulata. The currently sold sandarac was compared with the Tetraclinis articulata references, and with resins from the genera Agathis, Juniperus and Callitris, but its botanical source was not revealed.
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页数:10
相关论文
共 77 条
[61]   Natural resins and balsams from an eighteenth-century pharmaceutical collection analysed by gas chromatography/mass spectrometry [J].
Steigenberger, Gundel ;
Herm, Christoph .
ANALYTICAL AND BIOANALYTICAL CHEMISTRY, 2011, 401 (06) :1771-1784
[62]   Japanning in Spa at the End of the Seventeenth Century to the Middle of the Eighteenth Century: Historical Context and Materials for Lacquered bois de Spa [J].
Steyaert, Delphine ;
Decq, Louise ;
Cattersel, Vincent ;
Van Binnebeke, Emile ;
Indekeu, Charles ;
Fremout, Wim ;
Saverwyns, Steven .
STUDIES IN CONSERVATION, 2019, 64 (sup1) :S14-S30
[63]   Identification of the main constituents in sandarac resin, a natural gum base [J].
Sugimoto, Naoki ;
Kuroyanagi, Masanori ;
Kato, Takashi ;
Sato, Kyoko ;
Tada, Atsuko ;
Yamazaki, Takeshi ;
Tanamoto, Kenichi .
JOURNAL OF THE FOOD HYGIENIC SOCIETY OF JAPAN, 2006, 47 (02) :76-79
[64]   Characterisation and discrimination of various types of lac resin using gas chromatography mass spectrometry techniques with quaternary ammonium reagents [J].
Sutherland, K. ;
del Rio, J. C. .
JOURNAL OF CHROMATOGRAPHY A, 2014, 1338 :149-163
[65]  
Tingry P.- F., 1803, Traite theorique et pratique sur l'art de faire et d'appliquer les vernis
[66]  
sur les differents genres de peinture par impression et en decoration, ainsi que sur les couleurs simples et composees : accompagne de nouvelles observations sur le copal, de notes historiques sur la nature des matieres et sur les procedes mis en usage par les compositeurs de couleurs et de vernis et par les peintres, V2nd
[67]  
Van den Berg K.J., ICOM 200 12 TRIENNIA, V2, P855
[68]  
van den Berg K.J., 2002, P ART2002 NOND TEST
[69]  
van den Berg KJ, 2000, J MASS SPECTROM, V35, P512, DOI 10.1002/(SICI)1096-9888(200004)35:4<512::AID-JMS963>3.0.CO
[70]  
2-3