Nickel-Catalyzed Direct Alkylation of Terminal Alkynes at Room Temperature: A Hemilabile Pincer Ligand Enhances Catalytic Activity

被引:78
作者
Garcia, Pablo M. Perez [1 ]
Ren, Peng [1 ]
Scopelliti, Rosario [1 ]
Hu, Xile [1 ]
机构
[1] Ecole Polytech Fed Lausanne, Inst Chem Sci & Engn, Lab Inorgan Synth & Catalysis, EPFL ISIC LSCI, CH-1015 Lausanne, Switzerland
基金
瑞士国家科学基金会;
关键词
nickel; Sonogashira coupling alkynylation; pincer complex; kinetics; alkylation; BIMETALLIC OXIDATIVE ADDITION; GRIGNARD-REAGENTS; HALIDES; COMPLEXES; NI; ARYL; METHODOLOGY; BROMIDES; PD;
D O I
10.1021/cs501502u
中图分类号
O64 [物理化学(理论化学)、化学物理学];
学科分类号
070304 ; 081704 ;
摘要
Direct coupling of alkyl halides with terminal alkynes provides an efficient and streamlined access to alkyl-substituted alkynes, which are important synthetic intermediates, biologically active molecules, and organic materials. However, until now,there have been fewer than a handful of catalytic methods available for this reaction, and detailed mechanistic studies have not been reported. Herein, we describe the design and development a new nickel pincer complex that catalyzes the direct coupling of primary alkyl halides with terminal alkynes at room temperature. The catalysis has a good substrate scope and high functional group tolerance. Kinetic data suggest that the new pincer ligand is hemilabile, and the dissociation of a labile amine donor is the (t)urnover-determining step of the catalysis. An intermediate Ni-alkynyl species has been isolated and structurally characterized. The reactivity of this species gives insight into the nature of the active species for the activation of alkyl halide.
引用
收藏
页码:1164 / 1171
页数:8
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