A new version of a portable polonium source for the non-destructive PIXE (particle induced X-ray emission) analysis in the cultural heritage field

被引:9
作者
Romano, F. P. [1 ,2 ]
Pappalardo, L. [1 ,2 ]
Calvi, G. [3 ]
Costa, E. [2 ]
Marchetta, C. [2 ]
Pappalardo, G. [2 ]
Rizzo, F. [1 ,3 ]
Russo, S. [2 ]
机构
[1] CNR, Ist Beni Archeologici & Monumentali, I-95100 Catania, Italy
[2] Ist Nazl Fis Nucl, LANDIS, Lab Nazl Sud, I-95123 Catania, Italy
[3] Univ Catania, Dipartimento Fis & Astron, I-95123 Catania, Italy
关键词
PIXE; Non-destructive; Portable; Cultural heritage; ALPHA; SYSTEM; PIGMENTS; XRF;
D O I
10.1016/j.microc.2011.11.007
中图分类号
O65 [分析化学];
学科分类号
070302 ; 081704 ;
摘要
A new version of the portable polonium source, named L-PIXE (large-particle induced X-ray emission), to be used for the non-destructive analysis in the Cultural Heritage field, was realised in the framework of a collaboration between the Italian LNS-INFN (Laboratori Nazionali del Sud-Istituto Nazionale di Fisica Nucleare) and IBAM-CNR (Istituto per i Beni Archeologici e Monumentali-Consiglio Nazionale delle Ricerche). The new source presents a compact geometry and it was designed to operate with large area SDD (silicon drift detector) detectors. In particular, the L-PIXE source was coupled to a 50 mm(2) SDD detector and tested by measuring geochemical reference materials. Results evidenced a gain factor, in terms of counting statistics in the measured X-ray spectra, equal to 11-12 with respect to the previous versions of the source. A preliminary evaluation of the MDL (minimum detection limit) of the new experimental set-up evidenced the possibility of using the new L-PIXE source for identifying the presence of minor and, in some cases, trace elements composing samples under investigation. (C) 2011 Elsevier B.V. All rights reserved.
引用
收藏
页码:95 / 98
页数:4
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