Synthesis of sheathed carbon nanotube tips by the sol-gel technique

被引:16
作者
Brioude, A [1 ]
Vincent, P [1 ]
Journet, C [1 ]
Plenet, JC [1 ]
Purcell, ST [1 ]
机构
[1] Univ Lyon 1, CNRS, UMR 5586, LPMCN, F-69622 Villeurbanne, France
关键词
carbon nanotubes; TiO2; thin films; field emission; sol-gel;
D O I
10.1016/S0169-4332(03)00891-2
中图分类号
O64 [物理化学(理论化学)、化学物理学];
学科分类号
070304 ; 081704 ;
摘要
We describe the first elaboration of carbon nanotube tips (CN-tips) by the sol-gel technique. The CN-tips consist of single carbon nanotubes (CNs) or bundles sheathed by a nanometric layer of TiO2 fixed to the apex of a W base tip and oriented along its major axis. The straight-forward method potentially permits low cost batch fabrication. Structural analysis has been realized by transmission electron microscopy (TEM). These CN-tips are interesting for applications in applied surface science such as field emission (FE) sources and near field microscopy probes. A first field emission study has also been carried out showing that the TiO2 layer does not block FE. Relatively stable emission at voltages usual to FE from CNs at up to 0.8 muA current were obtained. (C) 2003 Elsevier B.V. All rights reserved.
引用
收藏
页码:4 / 9
页数:6
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