Preparation and characterization of belt-like Sb2Se3 crystals

被引：11

作者：

Han, Qiaofeng ^{[1
]}

Chen, Jian ^{[1
]}

Lu, Juan ^{[1
]}

Yang, Xujie ^{[1
]}

Lu, Lude ^{[1
]}

Wang, Xin ^{[1
]}

机构：

[1] Nanjing Univ Sci & Technol, Mat Chem Lab, Ctr Nanosci & Nanotechnol, Nanjing 210094, Peoples R China

来源：

MATERIALS LETTERS | 2008年 / 62卷 / 14期

基金：

中国国家自然科学基金;

关键词：

antimony selenium; hydrothermal treat; morphology;

D O I：

10.1016/j.matlet.2007.11.012

中图分类号：

T [工业技术];

学科分类号：

08 ;

摘要：

Orthorhombic Sb2Se3 belts are synthesized via a hydrothermal treatment at 200 degrees C and pH = 9-10 for 16 h. Transmission electron microscopic (TEM) images show that as-obtained Sb2Se3 belts are with a typical width in the range of 200-400 nm and length up to 20 mu m. High-resolution transmission electron microscopic (HRTEM) studies reveal that the Sb2Se3 are oriented in the [001] growth direction. The influences of poly vinyl alcohol (PVA) and the reaction conditions on the formation of belt-like Sb2Se3 microstructures are discussed. (C) 2007 Elsevier B.V. All rights reserved.

引用

页码：2050 / 2052

页数：3

共 13 条

[11] One-dimensional nanostructures: Synthesis, characterization, and applications
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[12] Polymer-controlled growth of hydrothermal Sb2Se3 nanoribbons via a process
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[J]. JOURNAL OF CRYSTAL GROWTH, 2003, 252 (04) : 570 - 574
[13] Pressure-controlled fabrication of stibnite nanorods by the solvothermal decomposition of a simple single-source precursor
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