4,4′-bipyridine acetic acid disolvate

被引：2

作者：

Ye, Ling ^{[1
]}

机构：

[1] Jilin Univ, State Key Lab Supramol Struct & Mat, Changchun 130012, Peoples R China

来源：

ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE | 2008年 / 64卷

关键词：

D O I：

10.1107/S1600536807062319

中图分类号：

O7 [晶体学];

学科分类号：

0702 ; 070205 ; 0703 ; 080501 ;

摘要：

The crystal structure of the title compound, C10H8N2 center dot 2C(2)H(4)O(2), is built up from 4,4'-bipyridine and acetic acid molecules linked by strong O-H center dot center dot center dot N hydrogen bonds. The 4,4'-bipyridine and the two acetic acid molecules are further connected through weak C-H center dot center dot center dot O hydrogen bonds to form a supramolecular two-dimensional network parallel to the ( 001) plane. The two pyridine rings make a dihedral angle of 31.8 (1)degrees.

引用

页码：O46 / U2903

页数：9

共 10 条

[1] Burnett M.N., 1996, ORTEP-III: Oak Ridge Thermal Ellipsoid Plot Program for Crystal Structure Illustrations
[2] DIA YM, 2005, ACTA CRYSTALLOGR E, V61, pO3919
[3] Farrugia L.J., 1997, J APPL CRYSTALLOGR, V30, P565
[4] 4,4′-Bipyridinium bis(3,5-dicarboxybenzoate) benzene-1,3,5-tricarboxylic acid hexahydrate
Li, XH
Lei, XX
Wang, S
[J]. ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2005, 61 : O1802 - O1804
[5] Layered structures formed by dinitrobenzoic acids
Pedireddi, VR
Ranganathan, A
Chatterjee, S
[J]. TETRAHEDRON LETTERS, 1998, 39 (52) : 9831 - 9834
[6] *RIG CORP, 1998, RAPID AUTO
[7] *RIG MSC INC, 2002, CRYSTALSTRUCTURE
[8] Sheldrick GM, 2015, ACTA CRYSTALLOGR C, V71, P3, DOI [10.1107/S2053229614024218, 10.1107/S0108767307043930]
[9] Single-crystal structure validation with the program PLATON
Spek, AL
[J]. JOURNAL OF APPLIED CRYSTALLOGRAPHY, 2003, 36 : 7 - 13
[10] WANG LZ, 2006, ACTA CRYSTALLOGR E, V62, pO3031

← 1 →