3-{[3-(4-Methoxyphenyl)-4,5-dihydro-1,2-oxazol-5-yl]methyl}-1,5-dimethyl-1H-1,5-benzodiazepine-2,4(3H,5H)-dione

被引：0

作者：

Dardouri, Rachida ^{[2
]}

Rodi, Yousef Kandri ^{[2
]}

Saffon, Natalie ^{[3
]}

Essassi, El Mokhtar ^{[4
]}

Ng, Seik Weng ^{[1
]}

机构：

[1] Univ Malaya, Dept Chem, Kuala Lumpur 50603, Malaysia

[2] Univ Sidi Mohamed Ben Abdallah, Lab Chim Organ Appl, Fac Sci & Tech, Fes, Morocco

[3] Univ Toulouse 3, Serv Commun Rayons X FR2599, Toulouse, France

[4] Univ Mohammed V Agdal, Lab Chim Organ Herocycl, Rabat, Morocco

来源：

ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE | 2011年 / 67卷

关键词：

D O I：

10.1107/S1600536811022872

中图分类号：

O7 [晶体学];

学科分类号：

0702 ; 070205 ; 0703 ; 080501 ;

摘要：

The molecule of the title compound, C22H23N3O4, features a benzodiazepine fused-ring system whose seven-membered ring adopts a boat-shaped conformation (with the C atoms of the fused-ring as the stern and the methine C atom as the prow). The methylene C atom connected to the methine C atom occupies an equatorial position. The methylene C atom is connected to the five-membered oxazole ring, both of which are disordered over two positions in a 0.634 (4):0.366 (4) ratio. Weak intermolecular C-H center dot center dot center dot O hydrogen bonding is present in the crystal structure.

引用

页码：O1729 / U1054

页数：11

共 50 条

[41] 2-[3-(4-Methoxyphenyl)-1-phenyl-1H-pyrazol-5-yl]phenol
Kausar, Rukhsana
Badshah, Amir
ul Haq, Muhammad Zia
Hasan, Aurangzeb
Bolte, Michael
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2009, 65 : O589 - U2416
[42] Synthesis of 1,3-dimethyl-2,4-dioxo-1H,2H,3H,4H-quinazolines and 1,5-dihydro-1,3-dimethyl-5-nitromethyl-2H-pyrano[4,3-d]pyrimidine-2,4(3H)-diones
Kostrub, Vladimir V.
Tsupak, Evgeny B.
Nelyubina, Yulia V.
MENDELEEV COMMUNICATIONS, 2009, 19 (04) : 220 - 221
[43] REDUCTION OF INACTIVATED CARBONYL-COMPOUNDS BY 1,5-DIHYDRO-PYRIMIDO[4,5-B]QUINOLINE-2,4(3H,10H)-DIONE (1,5-DIHYDRO-5-DEAZAFLAVIN)
YONEDA, F
SAKUMA, Y
NITTA, Y
CHEMISTRY LETTERS, 1978, (10) : 1177 - 1178
[44] 1-Benzyl-3-[(dimethylamino)methylene]-4-phenyl-1H-1,5-benzodiazepine-2(3H)-thione
Ballo, Daouda
Bouhfid, Rachid
Zouihri, Hafid
Essassi, El Mokhtar
Ng, Seik Weng
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2010, 66 : O1019 - U1313
[45] (Z)-3-(2-Methoxybenzyl)-1,5-benzothiazepin- 4(5H)-one
Selvakumar, R.
Bakthadoss, M.
Lakshmanan, D.
Murugavel, S.
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2012, 68 : O2126 - +
[46] (Z)-3-(2-Chlorobenzyl)-1,5-benzothiazepin-4(5H)-one
Sabari, V.
Selvakumar, R.
Bakthadoss, M.
Aravindhan, S.
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2012, 68 : O2283 - +
[47] 5-(4-Methoxyphenyl)-3-(4-nitrobenzyl-sulfanyl)-4,5-dihydro-3H-1,2,4-triazole
Qadeer, Ghulam
Rama, Nasim Hasan
Zareef, Muhammad
Li, Xin-Hua
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2007, 63 : O88 - O89
[48] 3-(4-Methoxyphenyl)-6,7-dihydro-1H-furo[3,4-c] pyran-4(3H)-one
Zhang, Jingyi
An, Ye
Zhang, Yikai
Shi, Guobing
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2012, 68 : O3451 - +
[49] Crystal structure of 5-(1-benzofuran-2-yl)-3-(4-methylphenyl)-4,5-dihydro-1,2-oxazol-5-ol
Ravi, A. J.
Vinayaka, A. C.
Jeyaseelan, S.
Sadashiva, M. P.
Devarajegowda, H. C.
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2015, 71 : O492 - U363
[50] 3-(3-Bromo-4-methoxyphenyl)-1,5-diphenylpentane-1,5-dione
Dutkiewicz, Grzegorz
Kumar, C. S. Chidan
Yathirajan, H. S.
Narayana, B.
Kubicki, Maciej
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2010, 66 : O816 - U2186

← 1 2 3 4 5 →