Synthesis of molybdenum disulfide particles by aerosol-assisted chemical vapor deposition

被引：6

作者：

Aleksandrov, S. E. ^{[1
]}

Filatov, K. D. ^{[1
]}

Tyurikov, K. S. ^{[1
]}

机构：

[1] Peter Great St Petersburg Polytech Univ, Ul Politekhnicheskaya 29-1, St Petersburg 195251, Russia

来源：

RUSSIAN JOURNAL OF APPLIED CHEMISTRY | 2016年 / 89卷 / 05期

基金：

俄罗斯科学基金会;

关键词：

ULTRASONIC SPRAY-PYROLYSIS;

D O I：

10.1134/S1070427216050050

中图分类号：

O69 [应用化学];

学科分类号：

081704 ;

摘要：

It was shown that dimethylformamide can be, in principle, used as a solvent of ammonium thiomolybdate for obtaining molybdenum disulfide particles by the aerosol-assisted chemical vapor deposition method. IR Fourier spectroscopy was used to examine (NH4)(2)MoS4-C3H7NO liquid solutions and the thermal stability of dimethylformamide and ammonium thiomolybdate vapors. It was demonstrated that pyrolysis at temperatures of 700-900A degrees C yields spherical molybdenum disulfide microparticles with average diameters in the range 0.6-1 A mu m and "onion" structure.

引用

页码：714 / 718

页数：5

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