4-Chloro-2-(6-nitro-1H-benzimidazol-2-yl)phenol N,N-dimethylformamide solvate

被引:1
|
作者
Farag, Abeer Mohamed [2 ]
Teoh, Siang Guan [2 ]
Osman, Hasnah [2 ]
Yeap, Chin Sing [1 ]
Fun, Hoong-Kun [1 ]
机构
[1] Univ Sains Malaysia, Sch Phys, Xray Crystallog Unit, George Town 11800, Malaysia
[2] Univ Sains Malaysia, Sch Chem Sci, George Town 11800, Malaysia
来源
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE | 2010年 / 66卷
关键词
D O I
10.1107/S1600536810041243
中图分类号
O7 [晶体学];
学科分类号
0702 ; 070205 ; 0703 ; 080501 ;
摘要
In the title compound, C(13)H(8)ClN(3)O(3)center dot C(3)H(7)NO, the benzimidazole and benzene rings make a dihedral angle of 0.63 (11)degrees. An intramolecular O-H center dot center dot center dot N hydrogen bond generates an S(6) ring motif. The solvent molecule is hydrogen-bonded to the benzimidazole molecule by intermolecular N-H center dot center dot center dot O and C-H center dot center dot center dot O hydrogen bonds, generating an R(2)(1)(7) ring motif. In the crystal, the molecules are arranged into parallel layers perpendicular to the c axis and stabilized by weak pi-pi interactions [centroid-centroid distances in the range 3.4036 (18)-3.5878 (16) angstrom].
引用
收藏
页码:O2863 / U593
页数:10
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