Rapid quantification of iron, copper and zinc in food premixes using energy dispersive X-ray fluorescence

被引：36

作者：

Perring, L ^{[1
]}

Andrey, D ^{[1
]}

Basic-Dvorzak, M ^{[1
]}

Hammer, D ^{[1
]}

机构：

[1] Nestec Ltd, Nestle Res Ctr, Dept Qual & Safety Assurance, CH-1000 Lausanne, Switzerland

来源：

JOURNAL OF FOOD COMPOSITION AND ANALYSIS | 2005年 / 18卷 / 07期

关键词：

EDXRF; ICP-AES; iron; copper; zinc; premixes; alternative; reference; quantitative analysis; rapids; minerals;

D O I：

10.1016/j.jfca.2004.06.011

中图分类号：

O69 [应用化学];

学科分类号：

081704 ;

摘要：

A simple and rapid method for the determination of iron, copper and zinc in food premixes (used during human food processing) by energy dispersive X-ray fluorescence (XRF) has been established and validated using 25 samples. Reference values were obtained by inductively coupled plasma-optical emission spectroscopy after microwave acidic digestions. Studied samples presenting wide ranges of concentrations: Fe = 500-35000 mg/kg, Cu = 50-4000 mg/kg and Zn = 700-32000 mg/kg were quantified in 200 s by XRF measurements using a rhodium tube. (c) 2004 Elsevier Inc. All rights reserved.

引用

页码：655 / 663

页数：9

共 9 条

[1] Vitamins and minerals:: A model for safe addition to foods
Flynn, A
Moreiras, O
Stehle, P
Fletcher, RJ
Müller, DJG
Rolland, V
[J]. EUROPEAN JOURNAL OF NUTRITION, 2003, 42 (02) : 118 - 130
[2] Hammer D, 2004, ATOM SPECTROSC, V25, P30
[3] HUGHES CG, 2002, XRAY FLUORESCENCE RA
[4] HUGHES CG, 2000, RAPID DETERMINATION
[5] Process analytical chemistry - future trends in industry
Kueppers, S
Haider, M
[J]. ANALYTICAL AND BIOANALYTICAL CHEMISTRY, 2003, 376 (03) : 313 - 315
[6] MEJIA LA, 1994, FOOD NUTR B, V19, P278
[7] Wavelength-dispersive x-ray fluorescence measurements on organic matrices: Application to milk-based products
Perring, L
Andrey, D
[J]. X-RAY SPECTROMETRY, 2004, 33 (02) : 128 - 135
[8] ED-XRF as a tool for rapid minerals control in milk-based products
Perring, L
Andrey, D
[J]. JOURNAL OF AGRICULTURAL AND FOOD CHEMISTRY, 2003, 51 (15) : 4207 - 4212
[9] ALTERNATIVES TO THE MEDIAN ABSOLUTE DEVIATION
ROUSSEEUW, PJ
CROUX, C
[J]. JOURNAL OF THE AMERICAN STATISTICAL ASSOCIATION, 1993, 88 (424) : 1273 - 1283

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