Preparation of bovine hydroxyapatite by transferred arc plasma

被引:28
作者
Yoganand, C. P. [1 ]
Selvarajan, V. [1 ]
Goudouri, O. M. [2 ]
Paraskevopoulos, K. M. [2 ]
Wu, Junshu [3 ]
Xue, Dongfeng [3 ]
机构
[1] Bharathiar Univ, Dept Phys, Plasma Lab, Coimbatore 641046, Tamil Nadu, India
[2] Aristotle Univ Thessaloniki, Dept Phys, Thessaloniki 54124, Greece
[3] Dalian Univ Technol, State Key Lab Fine Chem, Dept Mat Sci & Chem Engn, Sch Chem Engn, Dalian 116012, Peoples R China
关键词
Transferred arc plasma (TAP); Bovine bone; Hydroxyapatite; PHYSICOCHEMICAL CHARACTERIZATION; BONE; COATINGS; CERAMICS;
D O I
10.1016/j.cap.2010.11.035
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
Hydroxyapatite (Ca-10(PO4)(6)(OH)(2), abbreviated as HA) is a kind of bioactive material that has received considerable attention over the past decades as an implant material due to its excellent biocompatability for clinical applications. In this work, Hydroxyapatite was obtained by plasma processing of the natural bovine bones by Transferred arc plasma (TAP) processing at 5 kW in argon plasma for different processing times (i.e. 30, 45, 60, 90 and 120 s). The TAP synthesized HA bioceramic was characterized by XRD, FTIR, SEM-EDX and TG-DTA analysis. The effect of TAP processing time on the preparation of organic free HA from bovine bone was studied. The study indicated that TAP processing for 30, 45 and 60 s were insufficient for removal of organics from the natural bovine bone. Organic free bovine HA was obtained for 90 s TAP processing with a Ca/P ratio of 1.93 comparable with commercially available natural HA-Endobon powder. Whereas 120s of processing resulted in trivial thermal decomposition of HA in to its constituent phases. Thus our present investigation suggested that HA production from bovine bone using TAP processing is a time effective advantageous method in comparison to the annealing method. (C) 2010 Elsevier B.V. All rights reserved.
引用
收藏
页码:702 / 709
页数:8
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