3-Benzylidene-1′-methyl-4′-phenylcyclohexanespiro3′-pyrrolidine-2′-spiro-3"-indoline-2,2"-dione

被引:21
|
作者
Jeyabharathi, A
Ponnuswamy, MN
Raj, AA
Raghunathan, R
Razak, IA
Usman, A
Chantrapromma, S
Fun, HK [1 ]
机构
[1] Univ Sains Malaysia, Sch Phys, Xray Crystallog Unit, George Town 11800, Malaysia
[2] Univ Madras, Dept Crystallog & Biophys, Chennai 600025, India
[3] Univ Madras, Dept Organ Chem, Chennai 600025, India
[4] Prince Songkla Univ, Fac Sci, Dept Chem, Hat Yai, Songkhla, Thailand
关键词
D O I
10.1107/S1600536801013964
中图分类号
O7 [晶体学];
学科分类号
0702 ; 070205 ; 0703 ; 080501 ;
摘要
In the title compound, C30H28N2O2, there are two molecules in the asymmetric unit. In both molecules, the pyrrolidine ring adopts an envelope conformation whereas the conformation of the cyclohexane ring is half-chair. The oxindole moiety is almost perpendicular to the pyrrolidine ring; the benzylidene moiety and the phenyl ring are in equatorial and bisectional configurations with respect to their attached pyrrolidine and cyclohexanone rings, respectively. Intramolecular C-H . . .O and intermolecular N-H . . .N and N-H . . .O interactions stabilize the molecular structure and the packing in the crystal.
引用
收藏
页码:o901 / O903
页数:3
相关论文
共 50 条
  • [31] (4S)-4-(3,4-Dichlorophenyl)-1′-methyl-4′-phenyl-3,4-dihydronaphthalene-2-spiro-3′-pyrrolidine-2′-spiro-1"-acenaphthylene-1,2"(2H,1"H)-dione
    Murugan, R.
    Gunasekaran, B.
    Narayanan, S. Sriman
    Manivannan, V.
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2008, 64 : O1089 - U2281
  • [32] 1′-methyl-4′-phenylacenaphthene-1-spiro-2′-pyrrolidine-3′-spiro-2"-indan-2,1"3",-trione
    Govind, MM
    Selvanayagam, S
    Velmurugan, D
    Ravikumar, K
    Sureshbabu, AR
    Raghunathan, R
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2004, 60 : O547 - O549
  • [33] 5,7-dibromo-1′-methyl-2′-(4-methoxybenzoyl)-1H-indole-3-spiro-2′-pyrrolidine-3′-spiro-3"-1H-indole-2,2"(3H,3"H)-dione methanol solvate
    Seshadri, PR
    Selvanayagam, S
    Velmurugan, D
    Ravikumar, K
    Sureshbabu, AR
    Raghunathan, R
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2004, 60 : O550 - O552
  • [34] 1′-Methyl-4′-(1-naphthyl)-1H-indole-3-spiro-2′-pyrrolidine-3′-spiro-2"-thiazolo[3,2-a]-benzimidazole-2(3H),3"(2"H)-dione
    Zhang, Xiu-Ling
    Liu, Ai-Zhen
    Jin, Mei-Fang
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2006, 62 : O2961 - O2962
  • [35] 5-Benzylidene-1-phenyl-2",3"-dihydropiperidine-3-spiro-2′-pyrrolizidine-3′-spiro-3"-1H-indole-4,2"-dione
    Kumar, V. Vinodh
    Gayathri, D.
    Velmurugan, D.
    Ravikumar, K.
    Sridhar, Gowri
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2007, 63 : O2211 - O2212
  • [36] 5"-(4-Chlorobenzylidene)-1′,1"-dimethyl-3"-phenylacenaphthene-1-spiro-2′-pyrrolidine-3′-spiro-3"-pyridine-2,4"-dione
    Pandiarajan, S.
    Saravanamoorthy, S. N.
    Kumar, B. Ravi
    Kumar, R. Ranjith
    Athimoolam, S.
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2008, 64 : O99 - U3399
  • [37] 3-Benzylidene-3',7'-diphenylcyclohexanespiro-6'-(perhydro-2-thiapyrrolizidine)-5'-spiro-3''-1H-indole-2,2''-dione
    Subbiahpandi, A.
    Velmurugan, D.
    Ravikumar, K.
    Ramesh, E.
    Raghunathan, R.
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2006, 62 : O2259 - O2260
  • [38] Methyl 3-[ferrocenyl(hydroxy)methyl]-1-methyl-2′-oxospiro[pyrrolidine-2,3′-indoline]-3-carboxylate
    Kamala, E. Theboral Sugi
    Nirmala, S.
    Sudha, L.
    Kathiravan, S.
    Raghunathan, R.
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2009, 65 : M531 - U653
  • [39] 1′-Methyl-4′-(1-naphthyl)-1",2",3",4"-tetrahydroindane-2-spiro-2′-pyrrolidine-3′-spiro-2"-naphthalene-1,3,1"-trione
    Selvanayagam, S.
    Sridhar, B.
    Ravikumar, K.
    Saravanan, P.
    Raghunathan, R.
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2011, 67 : O629 - U1808
  • [40] 1-[(2-Chloro-3-quinolyl)methyl]indoline-2,3-dione
    Khan, F. Nawaz
    Roopan, S. Mohana
    Kone, Sriramakrishnaswamy
    Hathwar, Venkatesha R.
    Rauf, M. Khawar
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2010, 66 : O1141 - U684