2-butylamino-3-(4-fluorophenyl)-6,8-diphenyl-3,5,6,8-tetrahydro-4H-thiopyrano[4′,3′:4,5]thieno[2,3-d]pyrimidin-4-one

被引:0
作者
Li, Wen-Jing [1 ]
Li, Rong [1 ]
Wang, Wen-Qin [1 ]
Zhong, Ying [1 ]
机构
[1] Cent China Normal Univ, Minist Educ, Key Lab Pesticides & Chem Biol, Wuhan 430079, Peoples R China
来源
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS | 2007年 / 63卷
关键词
D O I
10.1107/S1600536807060850
中图分类号
O7 [晶体学];
学科分类号
0702 ; 070205 ; 0703 ; 080501 ;
摘要
In the title molecule, C31H28FN3OS2, the two fused rings of the thieno[ 3,2-d] pyrimidine group form a dihedral angle of 4.99 ( 12)degrees, and the benzene ring of the 4-fluorophenyl group forms a dihedral angle of 77.44 ( 15)degrees with the pyrimidine ring. The thiopyran ring is in a half-chair conformation. The crystal packing is stabilized by weak intermolecular C - H center dot center dot center dot N hydrogen bonds and weak pi-pi interactions with a centroid centroid distance of 3.900 ( 1) angstrom. The C atoms of the n-butyl group are disordered over two sites with approximate occupancies of 0.60 and 0.40.
引用
收藏
页码:O4869 / U6561
页数:13
相关论文
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