An Alternative Synthesis of 2,6-Dimethoxyl-1,4-Benzoquinone

被引：1
作者：
Wang, Qian [1 ]
Yang, Jian [1 ]
Zheng, Yang [1 ]
Liao, Xiali [1 ]
机构：
[1] Kunming Univ Sci & Technol, Fac Life Sci & Technol, 727 South Jingming Rd, Kunming 650500, Yunnan, Peoples R China
来源：
JOURNAL OF CHEMICAL RESEARCH | 2017年 / 41卷 / 04期
基金：
中国国家自然科学基金;
关键词：
2; 6-dimethoxy-1; 4-benzoquinone; aniline;
D O I：
10.3184/174751917X14894997017379
中图分类号：
O6 [化学];
学科分类号：
0703 ;
摘要：
An economic four-step synthesis of 2,6-dimethoxy-1,4-benzoquinone was achieved in 68% overall yield starting from aniline. The reaction sequence involved conversion to 1,3,5-tribromoaniline, deamination, methoxylation, and oxidation. The procedure is operationally simple and amenable to scale-up production.
引用
收藏
页码：193 / 194
页数：2
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