Reaction of 1,2-disilylbenzene with bis-[1,2-bis(dimethylphosphino)ethane]nickel(0). Isolation and characterization of the first silylnickel(IV) complex

被引:54
作者
Shimada, S [1 ]
Rao, MLN [1 ]
Tanaka, N [1 ]
机构
[1] Natl Inst Mat & Chem Res, Tsukuba, Ibaraki 3058565, Japan
关键词
D O I
10.1021/om980904h
中图分类号
O61 [无机化学];
学科分类号
070301 ; 081704 ;
摘要
The first silylnickel(IV) complex was isolated from the reaction of 1,2-disilylbenzene with a nichel(0) complex and characterized by multinuclear NMR and X-ray structure analysis. Bis(silyl)nickel(II) complexes, intermediates in the formation of the silylnickel(N) complex, were also characterized by NMR and/or X-ray analysis.
引用
收藏
页码:291 / 293
页数:3
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