The effect of intense plasma pulse pre-treatment on wettability in ceramic-copper system

被引:18
作者
Barlak, M. [1 ]
Piekoszewski, J.
Stanislawski, J.
Werner, Z.
Borkowska, K.
Chmielewski, M.
Sartowska, B.
Miskiewicz, M.
Starosta, W.
Walis, L.
Jagielski, J.
机构
[1] Andrzej Soltan Inst Nucl Studies, PL-05400 Otwock, Poland
[2] Inst Nucl Chem & Technol, PL-03145 Warsaw, Poland
[3] Polish Acad Sci, Inst Phys Chem, PL-01224 Warsaw, Poland
[4] Inst Elect Mat Technol, PL-01919 Warsaw, Poland
[5] Warsaw Univ Technol, Fac Engn & Mat Sci, Mat Design Div, PL-02507 Warsaw, Poland
关键词
carbon ceramics copper wetting; plasma pulses; PVD coatings;
D O I
10.1016/j.fusengdes.2007.08.010
中图分类号
TL [原子能技术]; O571 [原子核物理学];
学科分类号
0827 ; 082701 ;
摘要
The aim of the present work was to improve the wettability of ceramics such as pyrolytic graphite, glassy carbon, carbon-carbon composite and silicon carbide with liquid copper using three different processes. The first process consists in applying a high intensity plasma pulse (HIPP) in deposition by pulse erosion (DPE) mode to alloy a thin (nm scale) layer of Ti into the substrate. In the second process a thicker (mu m scale) layer of Ti is deposited by ArcPVD method. The third process is a sequential combination of the above processes. Samples were characterized by electron microscopy, X-ray fluorescence, X-ray diffraction, macroscopic photography and sessile drop tests. The best results were achieved for the third process. For 70% of the tests the contact angle between Ti layer and Cu droplets was in the range 20-70 degrees. (C) 2007 Elsevier B.V. All rights reserved.
引用
收藏
页码:2524 / 2530
页数:7
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