Chemical Fingerprint and Multicomponent Quantitative Analysis for the Quality Evaluation of Cyclocarya paliurus Leaves by HPLC-Q-TOF-MS

被引：53
作者：
Cao, Yanni [1 ]
Fang, Shengzuo [1 ,2 ]
Yin, Zhiqi [3 ,4 ]
Fu, Xiangxiang [1 ,2 ]
Shang, Xulan [1 ,2 ]
Yang, Wanxia [1 ,2 ]
Yang, Huimin [3 ,4 ]
机构：
[1] Nanjing Forestry Univ, Coll Forestry, Nanjing 210037, Jiangsu, Peoples R China
[2] Nanjing Forestry Univ, Coinnovat Ctr Sustainable Forestry Southern China, Nanjing 210037, Jiangsu, Peoples R China
[3] China Pharmaceut Univ, Dept Nat Med Chem, Nanjing 10009, Jiangsu, Peoples R China
[4] China Pharmaceut Univ, State Key Lab Nat Med, Nanjing 10009, Jiangsu, Peoples R China
来源：
MOLECULES | 2017年 / 22卷 / 11期
基金：
中国国家自然科学基金;
关键词：
Cyclocarya paliurus; fingerprint; HPLC-Q-TOF-MS; quantitative analysis; quality evaluation; PERFORMANCE LIQUID-CHROMATOGRAPHY; BATAL; ILJINSKAJA; FLAVONOID ACCUMULATION; CONSISTENCY EVALUATION; ANTIOXIDANT ACTIVITIES; PHENOLIC-COMPOUNDS; MASS-SPECTROMETRY; PLANT-EXTRACTS; POLYSACCHARIDE; L;
D O I：
10.3390/molecules22111927
中图分类号：
Q5 [生物化学]; Q7 [分子生物学];
学科分类号：
071010 ; 081704 ;
摘要：
Cyclocarya paliurus is an edible and medicinal plant containing various bioactive components with significant health benefits. A combinative method using high-performance liquid chromatography (HPLC) fingerprint and quantitative analysis was developed and successfully applied for characterization and quality evaluation of C. paliurus leaves collected from 18 geographical locations of China. For the fingerprint analysis, 21 common peaks were observed among the 18 samples, and these peaks were identified by high-performance liquid chromatography coupled with quadrupole time-of-flight mass spectrometry (HPLC-Q-TOF-MS), while a simultaneous quantification of 16 markers was conducted to interpret the variations of contents of these bioactive compounds among the C. paliurus leaves from different geographical locations. Quantification results showed that the contents of these sixteen investigated compounds varied greatly among the leaves from different locations. The developed new method would be a valuable reference for further study and development of this bioactive plant.
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页数：16
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