A simple device for the extraction of TLC spots: direct coupling with an electrospray mass spectrometer

被引:90
作者
Luftmann, H [1 ]
机构
[1] Univ Munster, Inst Organ Chem, Munster, Germany
关键词
TLC; extraction; electrospray mass spectrometry; ES;
D O I
10.1007/s00216-003-2293-3
中图分类号
Q5 [生物化学];
学科分类号
071010 ; 081704 ;
摘要
A new device is described which allows the recovery of compounds from thin layer chromatograms in short times, within a small volume, and without contamination. This apparatus can be coupled online to an electrospray mass spectrometer, but can also be used with other detectors or for micropreparations.
引用
收藏
页码:964 / 968
页数:5
相关论文
共 22 条
[1]  
Anderson RM, 1998, JPC-J PLANAR CHROMAT, V11, P336
[2]   Cellulose oligomers: preparation from cellulose triacetate, chemical transformations and reactions [J].
Arndt, P ;
Bockholt, K ;
Gerdes, R ;
Huschens, S ;
Pyplo, J ;
Redlich, H ;
Samm, K .
CELLULOSE, 2003, 10 (01) :75-83
[3]  
BUSCH K L, 1989, Journal of Planar Chromatography - Modern TLC, V2, P355
[4]   PLANAR CHROMATOGRAPHY COUPLED TO MASS-SPECTROMETRY [J].
BUSCH, KL ;
MULLIS, JO ;
CARLSON, RE .
JOURNAL OF LIQUID CHROMATOGRAPHY, 1993, 16 (08) :1695-1713
[5]  
CHRISTIE WW, 1990, LIPID TECHNOL, V2, P22
[6]  
CHRISTIE WW, 1999, LIPID TECHNOL, V11, P64
[7]  
CRECELIUS A, 2003, LCGC EUROPE APR, P2
[8]  
Esteban J, 1977, TEC LAB, V5, P285
[9]   THIN-LAYER CHROMATOGRAPHY MASS-SPECTROMETRY USING INFRARED-LASER DESORPTION [J].
FANIBANDA, T ;
MILNES, J ;
GORMALLY, J .
INTERNATIONAL JOURNAL OF MASS SPECTROMETRY AND ION PROCESSES, 1994, 140 :127-132
[10]  
Guittard J, 1999, RAPID COMMUN MASS SP, V13, P1838, DOI 10.1002/(SICI)1097-0231(19990930)13:18<1838::AID-RCM726>3.0.CO