Diagnostics of Carbonaceous Nanomaterial "Taunit" by Raman Spectroscopy

被引:1
作者
Maslova, O. A. [1 ]
Mikheykin, A. S. [1 ]
Leontiev, I. N. [1 ]
Yuzyuk, Yu. I. [1 ]
Tkachev, A. G. [2 ]
机构
[1] So Fed Univ, Fac Phys, Rostov Na Donu 344090, Russia
[2] Tambov State Tech Univ, Tambov, Russia
基金
俄罗斯基础研究基金会;
关键词
Multi-Walled Carbon Nanotubes; Raman Spectroscopy; Crystalline Structure Ordering; D- and G-Band Intensities Ratios; Pt-Catalyst Nanoparticles;
D O I
10.1166/jno.2012.1225
中图分类号
TM [电工技术]; TN [电子技术、通信技术];
学科分类号
0808 ; 0809 ;
摘要
Crystalline structure perfection of carbonaceous nanomaterial (CNM) "Taunir which constitutes the multi-walled nanotubes was studied using a Raman spectroscopy technique. CNM "Taunir was synthesized by MOCVD method. The pristine material, the samples annealed at different temperatures and the samples functionalized by Pt-catalyst nanoparticles were investigated. It has been found that "Taunir belongs to the poorly organized carbon materials but its crystalline structure was observed to order while the annealing temperature increased. D1 and G Raman band (at 1350 and 1580 cm(-1), respectively) intensity ratios were calculated to estimate the crystal structure ordering of CNM "Taunir. The investigation of the influence of functionalization by the catalyst nanoparticles shows that Pt-catalyst precipitation on the surface of MWNTs leads to the increase of the defect band intensity due to an appearance of lattice defects.
引用
收藏
页码:95 / 98
页数:4
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