Synthesis of Nickel Oxide Nanoparticles from Thermal Decomposition of a New Precursor

被引：36

作者：

Fereshteh, Zeinab ^{[3
]}

Salavati-Niasari, Masoud ^{[1
]}

Saberyan, Kamal ^{[2
]}

Hosseinpour-Mashkani, S. Mostafa

Tavakoli, Farnosh ^{[1
]}

机构：

[1] Univ Kashan, Inst Nano Sci & Nano Technol, Kashan, Iran

[2] Nucl Sci & Technol Res Inst, Nucl Fuel Cycle Res Sch, Tehran, Iran

[3] Isfahan Univ Technol, Dept Mat Engn, Esfahan, Iran

来源：

JOURNAL OF CLUSTER SCIENCE | 2012年 / 23卷 / 02期

基金：

美国国家科学基金会;

关键词：

Nanoparticles; Electron microscopy; FT-IR spectroscopy; Thermal decomposition; NIO; NANOCRYSTALS; COPPER; FILM;

D O I：

10.1007/s10876-012-0477-8

中图分类号：

O61 [无机化学];

学科分类号：

070301 ; 081704 ;

摘要：

Nickel oxide nanoparticles (25 nm) have been synthesized via decomposition of a new precursor nickel octanoate Ni(octa)(2) in the presence of oleylamine (C18H37N) and triphenylphosphine (C18H15P), in mild conditions. To control the particle size and morphology, combination of C18H15P and C18H37N were applied as surfactants. In this process, oleylamine was used as both the medium and the stabilizing reagent. C18H37N and C18H15P play an important role in preventing aggregation of NiO nanoparticles. The products were characterized by XRD, SEM, TEM, FT-IR, and TGA.

引用

页码：577 / 583

页数：7

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