L-lysine-Pd Complex Supported on Fe3O4 MNPs: a novel recoverable magnetic nanocatalyst for Suzuki C-C Cross-Coupling reaction

被引：17

作者：

Ashraf, Muhammad Aqeel ^{[1
,2
]}

Liu, Zhenling ^{[3
]}

Zhang, Dangquan ^{[1
]}

Alimoradi, Ashkan ^{[4
,5
]}

机构：

[1] Henan Agr Univ, Sch Forestry, Zhengzhou 450002, Peoples R China

[2] Univ Malaya, Dept Geol, Fac Sci, Kuala Lumpur 50603, Malaysia

[3] Henan Univ Technol, Sch Management, Zhengzhou 450001, Peoples R China

[4] Ton Duc Thang Univ, Dept Management Sci & Technol Dev, Ho Chi Minh City, Vietnam

[5] Ton Duc Thang Univ, Fac Appl Sci, Ho Chi Minh City, Vietnam

来源：

APPLIED ORGANOMETALLIC CHEMISTRY | 2020年 / 34卷 / 08期

关键词：

C-C coupling; Fe3O4@L-lysine-Pd; Nanocatalyst; reusable catalyst; Suzuki reaction; ONE-POT SYNTHESIS; EFFICIENT HETEROGENEOUS CATALYST; SULFUR-CONTAINING-COMPOUNDS; IONIC LIQUID; HIGHLY EFFICIENT; SULFONIC-ACID; MULTICOMPONENT SYNTHESIS; POLYHYDROQUINOLINE DERIVATIVES; MESOSTRUCTURED CATALYST; BOND FORMATION;

D O I：

10.1002/aoc.5668

中图分类号：

O69 [应用化学];

学科分类号：

081704 ;

摘要：

In this work, L-lysine-Pd Complex, immobilized onto the surface of Fe3O4 MNPs, was successfully prepared via simple and inexpensive procedure. The prepared nanocatalyst was considered as a robust and clean nano-reactor catalyst for the Suzuki and Heck C-C Cross-Coupling reactions in water as the green condition. This eco-friendly heterogeneous catalyst was characterized by Fourier transform infrared spectroscopy (FT-IR), X-Ray Diffractometer (XRD), energy-dispersive X-ray spectroscopy (EDS), inductively coupled plasma atomic emission spectroscopy (ICP), X-ray mapping, BET, thermogravimetric analysis (TGA), vibrating sample magnetometer (VSM), scanning electron microscopy (SEM) and Transmission electron microscopy (TEM) techniques. The use of a green medium, easy separation and workup, excellent reusability of the nanocatalyst and short reaction time are some outstanding advantages of this method.

引用

页数：18

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