Data-collection system for high-throughput X-ray absorption fine structure measurements

被引：3
作者：
Lu, Rui-You [1 ,2 ]
Gao, Qian [1 ]
Gu, Song-Qi [1 ]
Yang, Ya-Yun [1 ,2 ]
Si, Rui [1 ]
机构：
[1] Chinese Acad Sci, Shanghai Inst Appl Phys, Shanghai 201204, Peoples R China
[2] Univ Chinese Acad Sci, Beijing 100049, Peoples R China
来源：
NUCLEAR SCIENCE AND TECHNIQUES | 2016年 / 27卷 / 04期
基金：
中国国家自然科学基金;
关键词：
X-ray absorption fine structure; High throughput; Control system studio; Experimental physics and industrial control system; Graphical user interface; Data collection; FLUORESCENCE; SPECTROSCOPY; POLYMERIZATION; DIFFRACTION; BEAMLINE; SSRF;
D O I：
10.1007/s41365-016-0084-8
中图分类号：
TL [原子能技术]; O571 [原子核物理学];
学科分类号：
0827 ; 082701 ;
摘要：
A new X-ray absorption fine structure (XAFS) data-collection system based on the Experimental Physics and Industrial Control System software environment has been established at the BL14W1 beamline of the Shanghai Synchrotron Radiation Facility. The system provides for automatic sequential analysis of multiple samples for continuous high-throughput (HT) measurements. Specifically, 8 sample pellets are loaded into an alumina holder, and a high-precision two-dimensional translation stage is programmed to switch these samples automatically for collecting the XAFS spectrum of each sample in sequence. Experimenters implement HT measurements via a graphical user interface developed with Control System Studio. Finally, the successful operation of the HT XAFS system is demonstrated by running experiments on two groups of copper-ceria catalysts, each of which contains 8 different powder samples.
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页数：8
相关论文
共 20 条
  • [1] SLS Crystallization Platform at Beamline X06DA-A Fully Automated Pipeline Enabling in Situ X-ray Diffraction Screening
    Bingel-Erlenmeyer, R.
    Olieric, V.
    Grimshaw, J. P. A.
    Gabadinho, J.
    Wang, X.
    Ebner, S. G.
    Isenegger, A.
    Schneider, R.
    Schneider, J.
    Glettig, W.
    Pradervand, C.
    Panepucci, E. H.
    Tomizaki, T.
    Wang, M.
    Schulze-Briese, C.
    [J]. CRYSTAL GROWTH & DESIGN, 2011, 11 (04) : 916 - 923
  • [2] Dalesio L. R., 1991, P INT C ACC LARG EXP, P602
  • [3] Imaging polarimetry for high throughput chiral screening
    Gibbs, PR
    Uehara, CS
    Nguyen, PT
    Willson, RC
    [J]. BIOTECHNOLOGY PROGRESS, 2003, 19 (04) : 1329 - 1334
  • [4] Accelerating the living polymerization of 2-nonyl-2-oxazoline by implementing a microwave synthesizer into a high-throughput experimentation worknow
    Hoogenboom, R
    Wiesbrock, F
    Leenen, MAM
    Meier, MAR
    Schubert, US
    [J]. JOURNAL OF COMBINATORIAL CHEMISTRY, 2005, 7 (01): : 10 - 13
  • [5] Hu Z, 2014, NUCL SCI TECH, V25
  • [6] Jacky J., 2013, 14 INT C ACC LARG EX, P933
  • [7] Jia WH, 2015, NUCL SCI TECH, V26, DOI [10.13538/j.1001-8042/nst.26.20103, 10.13538/j.1001-8042/nst.26.020103]
  • [8] High-throughput microcoil NMR of compound libraries using zero-dispersion segmented flow analysis
    Kautz, RA
    Goetzinger, WK
    Karger, BL
    [J]. JOURNAL OF COMBINATORIAL CHEMISTRY, 2005, 7 (01): : 14 - 20
  • [9] High-throughput analysis in catalysis research using novel approaches to transmission infrared spectroscopy
    Leugers, A
    Neithamer, DR
    Sun, LS
    Hetzner, JE
    Hilty, S
    Hong, S
    Krause, M
    Beyerlein, K
    [J]. JOURNAL OF COMBINATORIAL CHEMISTRY, 2003, 5 (03): : 238 - 244
  • [10] Micro-X-ray fluorescence as a general high-throughput screening method for catalyst discovery and small molecule recognition
    Miller, TC
    Mann, G
    Havrilla, GJ
    Wells, CA
    Warner, BP
    Baker, RT
    [J]. JOURNAL OF COMBINATORIAL CHEMISTRY, 2003, 5 (03): : 245 - 252
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