Instrumentation for fast in-situ X-ray structure measurements on non-equilibrium liquids

被引:29
作者
Weber, J. K. R. [1 ,2 ]
Benmore, C. J. [2 ]
Jennings, G. [2 ]
Wilding, M. C. [3 ]
Parise, J. B. [4 ]
机构
[1] Mat Dev Inc, Arlington Hts, IL 60004 USA
[2] Argonne Natl Lab, Argonne, IL 60439 USA
[3] Aberystwyth Univ, Aberystwyth SY23 3BZ, Dyfed, Wales
[4] SUNY Stony Brook, Stony Brook, NY 11794 USA
关键词
X ray; Structure; Liquids; Glass; Extreme temperature; Supercooled;
D O I
10.1016/j.nima.2010.09.125
中图分类号
TH7 [仪器、仪表];
学科分类号
0804 ; 080401 ; 081102 ;
摘要
Probing the structure of non-equilibrium melts is important to advance the fundamental understanding of liquids and glass formation and development of new materials Combined use of high flux high energy X-rays and fast large area detectors enables in situ probing of liquids suspended and laser beam heated in an aerodynamic levitator High-energy X-rays provide high resolution data and avoid the complications of multiple scattering and absorption within the sample The use of non-contact processing heating and measurement enables deep supercooling and avoids the need for corrections due to scattering by the container The technique provides an extreme temperature sample environment for measurements at rates of 5 spectra per second from superheated and supercooled liquids (C) 2010 Elsevier BV All rights reserved
引用
收藏
页码:728 / 730
页数:3
相关论文
共 9 条
[1]   Two-dimensional detector software: From real detector to idealised image or two-theta scan [J].
Hammersley, AP ;
Svensson, SO ;
Hanfland, M ;
Fitch, AN ;
Hausermann, D .
HIGH PRESSURE RESEARCH, 1996, 14 (4-6) :235-248
[2]   Review of medical imaging with emphasis on X-ray detectors [J].
Hoheisel, M .
NUCLEAR INSTRUMENTS & METHODS IN PHYSICS RESEARCH SECTION A-ACCELERATORS SPECTROMETERS DETECTORS AND ASSOCIATED EQUIPMENT, 2006, 563 (01) :215-224
[3]   In situ high-energy X-ray diffraction study of the local structure of supercooled liquid Si -: art. no. 085501 [J].
Kim, TH ;
Lee, GW ;
Sieve, B ;
Gangopadhyay, AK ;
Hyers, RW ;
Rathz, TJ ;
Rogers, JR ;
Robinson, DS ;
Kelton, KF ;
Goldman, AI .
PHYSICAL REVIEW LETTERS, 2005, 95 (08)
[4]   Levitation apparatus for structural studies of high temperature liquids using synchrotron radiation [J].
Krishnan, S ;
Felten, JJ ;
Rix, JE ;
Weber, JKR ;
Nordine, PC ;
Beno, MA ;
Ansell, S ;
Price, DL .
REVIEW OF SCIENTIFIC INSTRUMENTS, 1997, 68 (09) :3512-3518
[5]   STRUCTURE AND DYNAMICS OF CAAL2O4 FROM LIQUID TO GLASS - A HIGH-TEMPERATURE AL-27 NMR TIME-RESOLVED STUDY [J].
MASSIOT, D ;
TRUMEAU, D ;
TOUZO, B ;
FARNAN, I ;
RIFFLET, JC ;
DOUY, A ;
COUTURES, JP .
JOURNAL OF PHYSICAL CHEMISTRY, 1995, 99 (44) :16455-16459
[6]   Structure of liquid SiO2:: A measurement by high-energy x-ray diffraction [J].
Mei, Q. ;
Benmore, C. J. ;
Weber, J. K. R. .
PHYSICAL REVIEW LETTERS, 2007, 98 (05)
[7]  
*NAT AC SCI, 2007, COND MATT MAT PHYS S, P221
[8]   Reciprocal-space instrumental effects on the real-space neutron atomic pair distribution function [J].
Qiu, XY ;
Bozin, ES ;
Juhas, P ;
Proffen, T ;
Billinge, SJL .
JOURNAL OF APPLIED CRYSTALLOGRAPHY, 2004, 37 :110-116
[9]   Acoustic levitator for structure measurements on low temperature liquid droplets [J].
Weber, J. K. R. ;
Rey, C. A. ;
Neuefeind, J. ;
Benmore, C. J. .
REVIEW OF SCIENTIFIC INSTRUMENTS, 2009, 80 (08)